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Method for measuring ultrafast laser absorptivity of powder material

A powder material and ultrafast laser technology, which is applied in the direction of measuring devices, analyzing materials, and material thermal development, etc., can solve the problem of large error in test values, inability to provide reference for ultrafast laser absorption rate testing, inaccurate test absorption rate, etc. problems, to achieve the effect of avoiding huge deviations

Pending Publication Date: 2022-02-18
BEIJING UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Chinese patent 202010107934.0 (disclosure date May 26, 2020) heats the material to a preset temperature by coil heating and then measures the laser absorptivity of the powder material at that temperature. However, this method ignores the effect of the laser and the thermal history of the material under coil heating. Different, the error of the test value is too large, which cannot provide reference for the test of ultrafast laser absorption rate
[0005] In order to solve the problems in the above-mentioned prior art, the present invention proposes the specific heat capacity test method of the powder material changing with temperature under ultrafast laser irradiation for the first time, and accurately obtains the specific heat capacity of powder material changing with temperature under ultrafast laser irradiation, and solves the problem of The problem of inaccurate test absorptivity caused by the large deviation between the specific heat capacity used in the test and the actual specific heat capacity is solved; according to the characteristics of the temperature change of the powder material in the ultrafast laser irradiation stage and the natural cooling stage, the functional relationship between the temperature change rate and temperature is proposed. The segmented fitting method avoids the error in the calculation of the absorption rate caused by the fitting deviation

Method used

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  • Method for measuring ultrafast laser absorptivity of powder material
  • Method for measuring ultrafast laser absorptivity of powder material
  • Method for measuring ultrafast laser absorptivity of powder material

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Embodiment 1

[0032] The present invention is used for testing the absorptivity test of femtosecond laser NbMoTaWZr mixed powder, and the specific embodiment is:

[0033] Step 100 starts the ultrafast laser absorptivity testing method of a powder material in the present invention.

[0034] Step 105 spread the NbMoTaWZr mixed powder in the crucible and place it in the vacuum chamber, set the laser power P=9W, irradiation time t=0.15s, repetition frequency f=750kHz, defocus h=35mm, pressure D= 4000Pa, so that all parts are in working condition.

[0035] Step 110 starts laser irradiation, uses a thermal imager to test the time-temperature data from the start of irradiation to the powder cooling to room temperature, and records the maximum temperature T of laser irradiation NbMoTaWZr mixed powder i1 = 119°C and the time t required for the temperature to cool down to room temperature after the laser irradiation is stopped i1 = 0.52s.

[0036] Step 115 Take the same volume of high-purity tungs...

Embodiment 2

[0050] The present invention is used for testing the absorptivity test of femtosecond laser alumina ceramic powder, and the specific implementation method is:

[0051] Step 100 starts the method for testing the ultrafast laser absorption rate of a powder material according to the present invention

[0052] Step 105 Spread the alumina ceramic powder in the crucible and place it in the vacuum chamber, set the laser power P=20W, irradiation time t=0.2s, repetition frequency f=1mHz, defocus h=15mm, pressure D =101kPa, make each part in working condition.

[0053] Step 110 starts laser irradiation, uses a thermal imager to test the time-temperature data from the start of irradiation to the cooling of the powder to room temperature, and records the maximum temperature T of the laser irradiation alumina ceramic powder i1 = 107°C and the time t required for the temperature to cool down to room temperature after the laser irradiation is stopped i1 = 2.12s.

[0054] Step 115 spread t...

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Abstract

The invention discloses a method for measuring the ultrafast laser absorptivity of a powder material and belongs to the field of ultrafast laser additive manufacturing. The invention provides a method for testing the specific heat capacity of the powder material along with the temperature change under ultrafast laser irradiation necessary for testing ultrafast laser absorptivity and a piecewise fitting method for the functional relationship between the temperature change rate and the temperature of the powder material under the action of the ultrafast laser for the first time, and achieve accurate measurement of absorptivity of the powder material under the action of ultrafast laser. The method is wide in application range and high in measurement precision, is suitable for actual measurement of the ultrafast laser absorptivity of various powder materials, fills the technical blank of the ultrafast laser absorptivity test of the powder materials, and provides precious basic data for engineering practice and scientific research.

Description

technical field [0001] The invention belongs to the technical field of ultrafast laser additive manufacturing, in particular to a method for measuring the ultrafast laser absorption rate of powder materials. Background technique [0002] At present, laser additive manufacturing generally faces problems such as molten pool instability, severe segregation, coarse grains, and low mechanical strength, which limit its wide application in industrial production, aerospace and other fields. This phenomenon is more pronounced in long-pulse-width lasers because the pulse width is greater than the electron-phonon coupling time and produces continuous thermal action. Compared with continuous laser and long pulse width laser, ultrafast laser has significant advantages in high precision, shape control and controllability in powder material additive manufacturing. Although ultrafast lasers have shown significant advantages and broad application prospects in the field of additive manufactu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N25/48
CPCG01N25/4846Y02P10/25
Inventor 季凌飞王昊张犁天
Owner BEIJING UNIV OF TECH
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