Process for preparing optical active chrysanthemic acid

An optically active and chrysanthemic acid technology is applied in the field of preparation of optically active chrysanthemic acid and can solve the problems of low yield of optically active chrysanthemic acid and the like
CN1373116AInactive Publication Date: 2002-10-09SUMITOMO CHEM CO LTD

Patent Information

Authority / Receiving Office
CN Β· China
Patent Type
Applications(China)
Current Assignee / Owner
SUMITOMO CHEM CO LTD
Publication Date
2002-10-09
Estimated Expiration
Not applicable Β· inactive patent
Patent Text Reader

Abstract

The invention discloses a preparation method of optically active chrysanthemum acid, which is characterized in that the ratio of the trans isomer is not less than 70% and the optical purity is 2%e.e.-less than 10%e.e. through the optical analysis of an optically active organic amine acid.
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Description

technical field

[0001] The invention relates to a preparation method of optically active chrysanthemic acid. Background technique

[0002] (+)-2,2-Dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylic acid, known as Chrysanthemum monocarboxylic acid, constitutes the acid component of synthetic pyrethroid insecticides.

[0003] The insecticidal activity of the trans-pyrethroids is generally higher than that of the cis-isomer. In particular, pyrethroids of (+)-trans-chrysanthemum monocarboxylic acid or chrysanthemic acid enriched in (+)-trans-chrysanthemum acid exhibit excellent insecticidal activity. Therefore, there has been a need for an industrially advantageous preparation of (+)-trans-chrysanthemic acid or enriched (+)-trans-chrysanthemic acid.

[0004] As a method for producing an optically active chrysanthemic acid derivative by using a synthetic technique, there is known a method in which (Β±)-trans-chrysanthemum monocarboxylic acid or trans-rich (Β±)-chrysanthmonoca...

Claims

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