Full history time-temperature indicator system
A temperature indicator, time technology, applied in the direction of testing time/temperature history, thermometer, device for measuring time interval, etc., can solve the problem of time-temperature indicator not providing direct measurement of time-temperature history process, etc.
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example 1
[0041] Preparation of Movable and Immobilized Reactants
[0042] The mobile reactant is 0.1M K in a mixture of 0.64% (w / w) alginate, 47.29% (w / w) glycerol, 52.06% (w / w) water 4 Fe(CN) 6 solution.
[0043] The immobilized reactants were prepared by dissolving 0.1M FeCl in a mixture of 47% (w / w) glycerol and 53% (w / w) water 3 The solution was slowly added to a mixture of 0.64% (w / w) alginate, 47.29% (w / w) glycerol, 52.06% (w / w) water. 0.1M FeCl 3 The amount of solution used was 17% (w / w) of the final weight. Mixing was accomplished by stirring vigorously at room temperature. In this way a viscous liquid is obtained which contains fixed Fe 3+ The small gel clusters are evenly distributed.
example 2
[0045] Time-temperature indicator prepared in ampoules
[0046] For the preparation of the ampoule-shaped time-temperature indicator, two transparent cylinders made of polyethylene are used, each of which is closed at one of its ends. The outer diameter of one of the cylinders (No. 1) is equal to the inner diameter of the No. 2 cylinder, so it fits into the other cylinder (No. 2).
[0047] Movable reactants were prepared according to the method described in Example 1 and contained K at a concentration of 0.1M 4 Fe(CN) 6 . The movable reactant is transferred to the No. 1 cylinder.
[0048] The method described in Example 1 is used to prepare the Fe-containing gel immobilized in the alginate gel. 3+ The immobilized reactants of the ions are then sent to the No. 2 cylinder.
[0049] The chemical reaction begins by assembling by gently pressing the two cylinders together, being careful to avoid the formation of air bubbles.
[0050] A time-temperature indicator was incubat...
example 3
[0052] In a ribbon time-temperature indicator, the color display is the time at 4°C The function
[0053] A time-temperature indicator was prepared as a strip wherein the reactants were prepared as described in Example 1 above.
[0054] For those containing fixed Fe 3+ The band-like time-temperature indicator displays the color of the portion being monitored. Color development was measured as the length of the dark blue region as a percentage of the total length of the portion of the time-temperature indicator containing the immobilized reactants. The time-temperature indicator maintains a constant temperature of 4°C for 76 days.
[0055] The results of the above experiments are shown in Table 3.1 below.
[0056] number of days
[0057] From the above results it is evident that the time-temperature indicator responds well to the exposure time at constant temperature.
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