Lithium anodes for electrochemical cells
An electrochemical and battery technology, applied in the field of lithium anode, can solve the problems of increasing the interface layer resistance, bad, changing the morphology of the deposited layer, etc.
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Embodiment 1
[0143] A vacuum web application system in a dry room with unrolled drive unit, liquid cooled drum, battery-carrying roll for tension control, rewind drive unit and two deposition zones loaded with 23 micron thick PET Anode substrate metallized with 100 nm copper on one side. Vacuum the deposition chamber to 10 -6 Torr. First, the thermally evaporated Li source is heated to 550 °C to generate a large amount of evaporation to deposit lithium on the substrate. The web drive was then turned on at a rate of 1.2 feet per minute. The lithium evaporation was stabilized to form an 8 micron lithium layer (PET / Cu / Li) on the copper of the base layer. Raise the DC magnetron cathode sputtering source region behind the lithium source to 2.4m Torr while only raising the lithium evaporation region to 10 -5 torr. The power of the cathode sputtering source was 2kW, and copper was deposited on top of the lithium layer with a thickness of 120, 60 or 30nm to form a composite anode PET / Cu / Li / Cu...
Embodiment 2
[0147] Three copper-protected lithium anodes were made by applying copper to the lithium surface of a PET / copper / lithium anode structure as described in Example 1. The thickness of the copper layer applied on the lithium outer surface was 30, 60 and 120 nanometers. These copper-protected lithium anodes were stored overnight at room temperature.
[0148] A lithium anode protected by copper (PET / copper / lithium / copper) or an uncoated PET / copper / lithium anode was used as a comparison, and a flat small battery was assembled with the fabricated cathode prepared by , a mixture of the following components was applied to one side of an aluminum foil substrate (Product No. 60303, available from Rexam Graphics, South Hadley, Massachusetts) coated with 17 micron thick conductive carbon: 75 parts elemental sulfur (available from Aldrich Chemical Company, Milwaukee, WI), 15 parts of conductive carbon pigment PRINTEXXE-2 (trademark for carbon pigments, available from Degussa Corporation, Ak...
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