High performance silicon emulsion and its preparation
A technology of silicone-acrylic emulsion and production method, which is applied in the field of silicone-acrylic emulsion and its production, and can solve problems such as unfavorable environmental protection
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[0065] Example 1. Polymerization of Seed Emulsion
[0066] Put 800Kg of deionized water, 0.5Kg of disodium hydrogen phosphate, 52Kg of sodium lauryl sulfate, 3.6Kg of ammonium persulfate into the reaction pot, add 139Kg of methyl methacrylate and 4.5Kg of methacrylic acid under stirring conditions , Primary dodecyl mercaptan 0.4Kg, after stirring for 30 minutes, start to heat up to 65-77℃, stop heating, blue light appears in the emulsion, exothermic reaction occurs in the reaction system, the temperature rises to 80-85℃, keep the temperature at 80 -82°C, constant temperature reaction for 30 minutes, the viscosity of the obtained seed emulsion is about 600mPa·s, the glass transition temperature Tg is 12, and the molecular weight is about 340.
Example Embodiment
[0067] Example 2. Polymerization of Seed Emulsion
[0068] Add 700Kg of deionized water, 1Kg of sodium dihydrogen phosphate, 45Kg of sodium lauryl sulfate, 35Kg of nonylphenol polyvinyl ether, and 8.6Kg of dicumyl peroxide into the reaction pot. Add acrylic acid under stirring conditions. Ester 194Kg, methacrylic acid 14.4Kg, t-dodecyl mercaptan 2Kg, after stirring for 30 minutes, the temperature began to rise to 65-77°C, the heating was stopped, blue light appeared in the emulsion, exothermic reaction occurred in the reaction system, and the temperature rose to 80 -85°C, keeping the temperature at 80-82°C, and reacting at a constant temperature for 30 minutes. The viscosity of the obtained seed emulsion is about 800mPa·s, the glass transition temperature Tg is 8, and the molecular weight is about 190.
Example Embodiment
[0069] Example 3. Polymerization of Seed Emulsion
[0070] Add 900Kg of deionized water, 0.1Kg of sodium bicarbonate, 7Kg of nonylphenol polyvinyl ether, 20Kg of alkylphenol polyvinyl ether phosphate, and 1.9Kg of potassium persulfate into the reaction pot, and add methacrylic acid under stirring. Methyl ester 65Kg, acrylic acid 5Kg, and primary lauryl mercaptan 1Kg. After stirring for 30 minutes, the temperature began to rise to 65-77°C, and the heating was stopped. Blue light appeared in the emulsion, exothermic reaction occurred in the reaction system, and the temperature rose to 80-85. ℃, keep the temperature at 80-82℃, and react at a constant temperature for 30 minutes. The viscosity of the obtained seed emulsion is about 400 mPa·s, the glass transition temperature Tg is 14, and the molecular weight is about 260.
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