Biodegradable lubricants
A biodegradable and lubricant technology, used in the field of synthetic ester lubricants, can solve the problems of lubricants accumulated on the water surface and cannot be used in environmentally sensitive applications.
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Embodiment 1
[0039] The preparation method comprises the following steps:
[0040] 1) Add all of the overbased calcium sulfonate to the kettle and heat with stirring to bring the temperature of the mixture to 160-185°F (71.1-85.0°C).
[0041] 2) Add 35-45% of PE-C to the kettle 5-10 Esters and water equivalent to 3-5% of the total feed. Stir and allow the temperature of the mixture to return to 160-185°F (71.1-85.0°C).
[0042] 3) Add all linear alkylbenzene sulfonic acid dissolved in all isopropanol.
[0043] 4) 10-15 minutes after the above three components are mixed into the kettle, add all the acetic acid.
[0044] 5) Continue heating slowly (to 210-215°F (98.9-101.7°C) over 30-60 minutes) with agitation, then begin full heating.
[0045] 6) When the temperature of the mixture reaches 235-250°F (112.8-121.1°C), if the mixture has begun to thicken, add Tech-PE-C 5-10 Esters (about 20% of the total).
[0046] 7) When the temperature of the mixture reaches 235-250°F (112.8-12...
Embodiment 2
[0054] test description
[0055] According to the OECD test, the biodegradability of oil is 69.2%.
Embodiment 3
[0058] Preparation:
[0059] 1) Add all of the overbased calcium sulfonate to the kettle and heat with stirring to bring the temperature of the mixture to 160-185°F (71.1-85.0°C).
[0060] 2) Add 35-45% of the total amount of DiPE-C to the kettle 5 C 8 / 10 ester and add water until it reaches 3-5% of the total dosage. With stirring, allow the temperature of the mixture to return to 160-185°F (71.1-85.0°C).
[0061] 3) Add all linear alkylbenzene sulfonic acid dissolved in all isopropanol.
[0062] 4) 10-15 minutes after the above three components are mixed into the kettle, add all the acetic acid.
[0063] 5) Continue to heat slowly while stirring (heat to 210-215°F (98.9-101.7°C) over 30-60 minutes), then begin to heat thoroughly.
[0064] 6) When the temperature of the mixture reaches 235-250°F (112.8-121.1°C), if the mixture has begun to thicken, add DiPE-C 5 C 8 / 10 Esters (about 20% of the total).
[0065] 7) When the temperature of the mixture reaches 235-25...
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