Preparation of gardenia jasminoides by membrane separation technology
A gardenia extract, membrane separation technology, applied in the direction of membrane technology, semipermeable membrane separation, carboxylate preparation, etc., can solve the problems of difficult storage, easy moisture absorption of products, etc., to reduce production costs, improve separation and purification efficiency, Effect of improving yield and quality
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0034] Use gardenia produced in Fujian as the raw material, wash fresh gardenia with water, dry (air-dried, oven-dried or sun-dried), pulverize, and pass through a 20-30 mesh sieve to obtain gardenia powder, and put 2.9kg of gardenia powder into the extraction tank 40% methanol-acetone (1:1) aqueous solution with 10 times the dry weight (W / W) of gardenia powder, refluxed extraction at 68°C for 3 times, each time for 2 hours, combined extracts, filtered, Under the conditions of -0.06~-0.095MPa and 50~80°C, the filtrate is recovered under reduced pressure to recover the solvent, and then concentrated in vacuo to obtain the gardenia extract. After determination, the extraction rates of gardenia iridoid glycosides, carotenoids and chlorogenic acid were 93.2%, 96.3% and 93.1%, respectively.
[0035] Next, the crude extract of Gardenia jasminoides is first added with an appropriate amount of water and stirred into a suspension to make the specific gravity of the suspension reach 1.0...
Embodiment 2
[0037] Put 2.6 kg of gardenia powder of 20 to 30 meshes into an extraction tank, extract 2 times at 50°C with 25% aqueous methanol solution of 15 times the dry weight (W / W) of gardenia powder, each time for 3 hours, and combine The extract is filtered, and the filtrate is recovered under reduced pressure under the conditions of -0.06 to -0.095MPa and 50 to 80°C, and concentrated in a vacuum to form a gardenia extract. After determination, the extraction rates of gardenia iridoid glycosides, carotenoids and chlorogenic acid were 92.3%, 92.8% and 91.8%, respectively.
[0038] Stir the gardenia crude extract with appropriate amount of water to form a suspension, so that the specific gravity of the suspension reaches 1.12, and then use a polyvinylidene fluoride membrane with a molecular weight cut-off of 30,000 to perform membrane separation and removal of impurities at 0.60 MPa to remove proteins, polysaccharides and other After the macromolecular impurities are removed, the gard...
Embodiment 3
[0040] Put 2.7 kg of gardenia powder of 20 to 30 meshes into an extraction tank, use 75% aqueous methanol solution of 5 times the dry weight (W / W) of gardenia powder, extract under reflux at 80°C for 1 hour, filter, and the filtrate is in- Under the conditions of 0.06~-0.095MPa and 50~80°C, the solvent is recovered under reduced pressure, and the gardenia extract is obtained by vacuum concentration. After determination, the extraction rates of gardenia iridoid glycosides, carotenoids and chlorogenic acid were 95.6%, 95.0% and 93.5%, respectively.
[0041] Stir the gardenia crude extract with appropriate amount of water to form a suspension, so that the specific gravity of the suspension reaches 1.03, and then use an inorganic ceramic membrane with a membrane pore size of 0.22 μm to perform membrane separation and removal of impurities at 0.25 MPa to remove macromolecules such as proteins and polysaccharides After removing the impurities, the Gardenia jasmine extract after memb...
PUM
Property | Measurement | Unit |
---|---|---|
Membrane pore size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com