Forecasting method for isothermal crystal dynamics parameter of high polymer
A kinetic parameter, isothermal crystallization technology, applied in measurement devices, scientific instruments, electrical digital data processing, etc., can solve the problem that high polymers have not been reported yet.
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[0054] The method for obtaining the initial linear rate of crystallization G(0) is: melt the sample on the electric heating plate for 7 minutes, then quickly transfer it to a hot stage at a set temperature to crystallize it, observe the crystal form, and measure the linear growth of the sample at this temperature rate, draw the linear growth rate-time curve, and derive the initial crystallization linear rate.
[0055] The method for obtaining the initial number of crystal nuclei is as follows: put the sample on a glass slide, melt it for 7 minutes, close the cover glass and press it into a thin film, quickly put it into an oil bath with a constant crystallization temperature, keep the temperature at a constant temperature for 5 hours, and take it out naturally. Cool down to room temperature, observe and take pictures under a transmission polarizing microscope; estimate the number of spherulites in the simulation system according to the pictures, the steps are as follows: use a ...
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