Triacetin resistant hot melt adhesive
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[0032] All adhesive formulations were prepared using a single blade mixer at temperature of 300° F. The adhesives were then subjected to the following tests.
[0033] Viscosity of hot melt adhesives was measured using a Brookfield Thermalsel viscometer with a number 27 spindle. The Gardner color of the hot melt adhesive was measured at 250° F., at which the adhesive was molten.
[0034] Adhesive bonds were made using a ¼ inch bead width on non-porous plug wrap paper substrates with dimension of 2 inch wide and 3 inch long. Adhesion was determined by aging the adhesive bonds at various temperature for 24 hr and then separating the bonds immediately. The resulting percentage of fiber tear (FT) was recorded.
[0035] In determination of triacetin resistance, the adhesives bonds were soaked in triacetin for 24 hr at ambient temperature and then were separated immediately. The relative bond strength and the resulting fiber tear were recorded. Triacetin resistance is determined to be good if mo...
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