127 results about "Ixeris" patented technology

The invention discloses a fermented preparation method of vegetables, belonging to the field of vegetable deep processing, in particular to the field of vegetable fermented processing. The method comprises the following steps of: (1) adding materials and sealing; (2) carrying out primary fermentation; (3) fermenting after regulating temperature; and (4) seasoning. The fermented preparation method of vegetables is characterized in that: in the step of fermenting after regulating the temperature, fermentation is carried out after the temperature is controlled to be 15-30 DEG C for 30-90 hours, and meantime, the temperature is dropped to 0-5 DEG C at least once and maintained for 1-10 hours. In the invention, the fermentation is carried out via lactic acid bacteria, thus herba ixeris products have good flavor and are easy to store and eat, and the products are rich in probiotics and various nutrient components. When the method is used for producing herba ixeris pickles, manufacturers do not need to specially cultivate fermentation bacteria and build related cultivation equipment and facilities, thereby saving personnel and equipment investments.

The invention discloses a compound traditional Chinese medicine for diminishing inflammation, checking diarrhea and relieving pain. The compound traditional Chinese medicine consists of the following active pharmaceutical ingredients by weight:10-14 grams of poria, 8-12 grams of rhizoma atractylodis macrocephalae, 10-14 grams of semen dolichoris album, 8-12 grams of dioscorea opposita, 6-10 grams of myristica fragrans, 10-14 grams of cortex magnoliae officinalis, 8-12 grams of rhizoma atractylodis, 8-12 grams of endoconcha sepiae, 6-10 grams of pericarpium citri reticulatae, 4-8 grams of pinellia tuber, 8-12 grams of inula britannica, 8-12 grams of reddle, 8-12 grams of endothelium corneum gigeriae galli, 8-12 grams of fructus amomi, 8-12 grams of fructus crataegi, 8-12 grams of fructus hordei germinatus, 8-12 grams of semen raphani, 6-10 grams of massa medicata fermentata, 8-12 grams of root of pilose asiabell, 8-12 grams of ixeris denticulata, 8-12 grams of anemone chinensis, 8-12 grams of herba taraxaci, 6-10 grams of fructus litseae, 4-8 grams of lignum dalbergiae odoriferae, 4-8 grams of cortex fraxini, 4-8 grams of pericarpium granati, 8-12 grams of halloysit, 4-8 grams of citrus medica linn, 4-8 grams of fructus citri sarcodactylis, 6-10 grams of corydalis turtschaninovii bess and 6-10 grams of fructus meliae toosendan. The compound traditional Chinese medicine has obvious effects in treating chronic gastritis, dyspepsia, diarrhea and abdominal pain. The compound traditional Chinese medicine has the advantages of short treatment time, good treatment effect, no side effect and the like.

The invention relates to a compound traditional Chinese medicine liquid foliar fertilizer and a production method thereof. The production method of the compound traditional Chinese medicine liquid foliar fertilizer comprises the steps of: mixing three or more out of the following traditional herbal medicines: pinellia ternata, herba seu radix cirsii japonici, moon valley green, rumex patientia l., datura, fructus meliae toosendan, annual artemisia, bidens tripartita l, drug sweetflag rhizome, spanish needles herb, Chinese ixeris herb, herba taraxaci, virgate wormwood, chinese stellera root, euphorbia fischeriana, artemisia scoparia and season radix euphorbiae lantu with three or more of the following acidic solvents: tri-n-butyl borate, selenious acid, sodium selenite, methyl salicylate, sterile crystal sulfanilamide, niflumic acid, ethyl acetate, sulindac, monopotassium phosphate, ammonium sulfate, mefenamic acid and zinc sulfate into mixed a 100 DEG C hot water solution, and carrying out soaking, grinding and pulping, filtering and clarifying to obtain the compound traditional Chinese medicine liquid foliar fertilizer. The compound traditional Chinese medicine liquid foliar fertilizer is a botanical pesticide, and has toxic effect of organic insecticide and bactericide and compound liquid preparation of acidic nutrient element fertilizer.

The invention relates to a method for simultaneously determining contents of 10 nucleoside components in sowthistle-leaf ixeris seedling injection by utilizing an HPLC-DAD (High Performance Liquid Chromatography-Diode Array detector) method, and belongs to the field of traditional Chinese medicine component analysis. The method comprises the following steps of: (1) preparation of a mixed reference liquid; (2) preparation of a test liquid; and (3) determining method: precisely absorbing the mixed reference liquid and the test liquid respectively by the HPLC-DAD method, injecting to a detector and detecting, wherein the chromatographic condition is as follows: the chromatographic column is DiamonsilC18(2), the detection wavelength is 260nm, the flow rate is 1mL/min, the column temperature is 35 DEG C, the sample size is 10 microlitres, and the gradient elute condition is 0-5 minutes; performing gradient eluting based on 2% of acetonitrile by volume fraction; linearly increasing to 9% of acetonitrile with 5-9 minutes; linearly increasing to 11% of acetonitrile with 9-15 minutes; and linearly increasing to 40% of acetonitrile with 15-25 minutes. The method for simultaneously determining the contents of the 10 nucleoside components in sowthistle-leaf ixeris seedling injection established by the invention is simple in analytic method, good in repeatability and accurate and reliable, and can provide reference for quality control of the sowthistle-leaf ixeris seedling injection.

The invention discloses a research for realizing quick classification and identification of chemical components in an ixeris sonchifolia hance injection based on a UPLC-Q-TOF-MS technology, and aims to take flavonoids, organic acids, amino acids and nucleosides in the ixeris sonchifolia hance injection as research objects to realize quick classification and identification of the chemical components in the ixeris sonchifolia hance injection based on a UPLC-Q-TOF-MS technical platform. The research comprises the following steps: firstly, performing information integration on components of flavonoids, organic acids, amino acids and nucleosides in the ixeris sonchifolia hance injection to discover and summarize a rule for diagnosing fragments and neutral losses of the four types of substances; meanwhile, performing mass spectrographic analysis on reference substances of different types of compounds by adopting the UPLC-Q-TOF-MS technology, and performing verification; and constructing a method for realizing quick classification and identification of chemical components in the ixeris sonchifolia hance injection by using a method for diagnosing fragments and neutral losses as a screening and identifying tool.

The invention relates to a method for measuring contents of six amino acids in an ixeris sonchifolia injection by using a pre-column derivatization method, belonging to the field of traditional Chinese medicine ingredient analysis. The method comprises the following steps: (1) preparing a mixed reference substance solution containing 217.0mg.L<-1> of proline, 37.40mg.L<-1> of alanine, 44.40mg.L<-1> of valine, 39.80mg.L<-1> of isoleucine, 43.20mg.L<-1> of leucine and 42.20mg.L<-1> of phenylalanine; (2) preparing a solution of test articles; and (3) carrying out gradient elution according to the following chromatographic conditions: a DiamonsilC18(2) chromatographic column (200*4.6mm, 5mu m), 25 DEG C of column temperature, 350nm of detection wavelength, 1.0mL/min of flow velocity, 10mu L of sample amount, a mobile phase A, namely water, a mobile phase B, namely 30mmol/L NaAc (containing 1% of N,N-dimethylfomamide), 6.40 of pH value and a mobile phase C, namely acetonitrile. The method has the advantages of simplicity, convenience, easiness in operation, high accuracy, good repeatability and the like and lays the foundation for research of the quality control method of the ixeris sonchifolia injection.

A general ixeris flavone containing luteolin-7-0-beta-D-phranoglucuronide (C21H18O12), a freeze-dried powder injection prepared from said general ixeris flavone, mannitol and the water for injection, and the preparing process and quality control method of said freeze-dried powder injection are disclosed.

A kudiezi medicinal preparation for treating cerebrovascular and ophthalmology diseases, wherein the medicinal preparation includes kudiezi spray-drying powder injection, high capacity fluid infusion, injection, tablet, capsule, granula, oral liquid, pill. The process for making the preparation can be realized by the conventional preparation process, or by the nano techniques.

The present invention discloses the application of Ixeris Sonchifolia Hance flavone compounds in preparing medicine for treating coronary heart disease, and the extraction process of Ixeris Sonchifolia Hance flavone compounds and five monomer compounds. Ixeris Sonchifolia Hance flavone compounds applied in medicine for treating coronary heart disease has the features of low toxic side effect, determined curative effect, safety and reliability. The medicine has no negative reactions of bleeding, allergy, causing hypertension, etc.

The invention relates to a method for simultaneously determining five organic acid components content in a Ixeris sonchifolia Hance injection by HPLC-DAD method, which comprises the following steps: 1)preparing a mixed reference substance solution; 2)preparing a tested object solution; 3) using a HPLC-DAD method, wherein the chromatogram condition is characterized in that a chromatographic column is Diamonsil c18 (2), the column temperature is 40 DEG C, the detection wavelength is 325nm, the flow velocity is 1mL.min<-1>, the sample size is 10mumL; the mobile phase is acetonitrile and 0.1% of formic acid water, the gradient elution condition is characterized in that 9% of acetonitrile linearity is increased to 11% for 0-15 minutes, and is increased to 18% for 15-16 minutes, is increased to 20% for 16-30 minutes, and then increased to 49% for 30-40 minutes. The analysis method of five organic acid components content in Ixeris sonchifolia Hance injection has the advantages of rapid determination, good repeatability, accurate result and good stability, and can be used for controlling the quality of the Ixeris sonchifolia Hance injection.

The invention provides feed for laying ducks and a preparation method thereof, and belongs to the technical field of feed for ducks. The feed comprises corn, soybean meal, soya bean lecithin, queen bee larvae freeze-dried powder, beer yeast powder, vinasse, vinegar tortoise plastron, cuttle bones, all-grass of Chinese ixeris, herba leonuri, herbs of nutgrass galingale, lycopus lucidus, folium isatidis, gynostemma pentaphyllum, yerbadetajo herbs, herba portulacae, garlic, yam peels, expanded blood meal, eels, ground beetles, salt, calcium hydrophosphate, traditional Chinese medicine concentrated powder, compound enzymes, multivitamins and compound trace elements. The traditional Chinese medicine concentrated powder is obtained through the steps that even mixing is conducted on, by weight, 3-7 parts of milkvetch roots, 1-3 parts of angelica sinensis, 1-3 parts of panax notoginseng, 2-5 parts of radix ophiopogonis, 3-7 parts of epimediums, 1-3 parts of rhizoma chuanxiong, 2-5 parts of rhizoma atractylodis macrocephalae, 3-7 parts of red peony roots, 2-5 parts of radix scutellariae and 3-7 parts of salviae miltiorrhizae, and extraction, concentration and drying are conducted on the mixture in sequence. According to the feed for the laying ducks and the preparation method thereof, by means of the feed for the laying ducks, the egg production quality of the laying ducks can be improved, and after feeding is conducted, the fertilization rate and the hatchability of duck eggs are high.

The invention discloses an injection made from Chinese herb Ixeris Sonchifolia Hance for treatment of cardio-cerebral vascular diseases and fundus diseases and method of producing thereof. The injection is in a form of lyophilized powder in which the rate of flavone to adenosine is 5 mg: 15 μg or 5 mg: 30 μg. The flavone and adenosine from Ixeris Sonchifolia Hance is more stable in the lyophilized powder form than in liquid form for injection so that it is easy to control the quality of the product so as to make the medicament safe and effective. It has benefit in store.

The invention discloses a freeze dried injection of seeding of autumnal sowthistle-leaf ixeris and preparation method, wherein the injection is prepared from seeding of autumnal sowthistle-leaf ixeris extract and medicinal adjuvant, the preparation consists of ultrasonic extraction, high speed centrifuging and ultrafiltrating the extract, disintegrating and purifying with polyamide resin columns.

The invention discloses a cultivation and quality control method for ixeris sonchifolia hance for Kudiezi injection, which is characterized by including seedling raising, transplanting, field management and harvesting. A method of quality control for ixeris sonchifolia hance is also studied and includes a method of colorimetric determination for large-class active ingredients such as flavone and total polyphenol in ixeris sonchifolia hance, and a method of multi-component quantitation by one marker for liquid gradient elution of cichoric acid, luteoline-7-O-beta-D-glucuronide and caftaric acid. By the technique of cultivation of ixeris sonchifolia hance, planting and harvesting of two crops a year are achieved, land resources are saved, yield per unit area is increased to 100%-150%, and quality of the ixeris sonchifolia hance meets the requirement of medicinal materials for traditional Chinese medicine injection.

The invention belongs to the field of analyzing Chinese herbal medicinal ingredients, and in particular discloses a method for rapid analysis of flavonoid glycoside and phenolic acid active ingredients in an ixeris sonchifolia injection by virtue of high performance liquid chromatography (HPLC). Chromatographic analysis conditions are as follows: (1) chromatographic column is a C18 reversed-phase chromatographic column; (2) a mobile phase consists of methanol, water, tetrahydrofuran and acid, and volume ratios of various ingredients in the mobile phases are as follows: the ratio of the tetrahydrofuran to the methanol is 0.03-0.1, the total proportion of the tetrahydrofuran and the methanol is 30-40% and the proportion of the acid is 0.1-2% of the water phase; (3) an ultraviolet detection wavelength is 348nm; and (4) chromatographic column temperature is 35-45 DEG C. Under an isocratic elution condition, more than 15 chromatographic peaks can be simultaneously separated and analyzed within 20min; compared with former methods, the method disclosed by the invention can be used for solving a problem that luteolin-7-O-beta-D-glucoside and luteolin-7-O-beta-D-glucuronide are difficult to separate, and the phenolic acid chromatographic peak in the ixeris sonchifolia injection can be better separated; and furthermore, analysis time is greatly shortened by the method.

The present invention discloses the preparation process of sowthistle-leaf ixeris injection, and features that purified sowthistle-leaf ixeris extract is first obtained by means of new purification process and then prepared into injection or mixed with medicinal supplementary material and prepared into freeze powder for injection. Pharmaceutical experiment results show that the sowthistle-leaf ixeris injection of the present invention has even high pharmaceutical effect.

The invention discloses a method for removing heavy metals (Pb, Zn, Cu, Cd and As) in plants by using different acids. The method is characterized in that heavy metals in dry matters of plants such as tobaccos, pastures (sudangrass, grain amaranth, endive, sowthistle-leaf Ixeris and rumex), vegetables and dreg cakes are extracted by using ethyl alcohol leach liquor of the acids as an extraction agent through vibration and rolling, so that the content of the heavy metals in the plants is reduced, the pollution to environments is reduced, and the food safety problem caused by excessive heavy metals is avoided.

The invention discloses a gel for promoting wound healing. The gel is mainly prepared from the following raw materials in parts by mass: 4-9 parts of flos buddlejae, 7-12 parts of ixeris sonchifolia hance, 8-16 parts of shepherdspurse herb, 8-14 parts of diverse wormwood herb, 5-10 parts of rhizoma nelumbinis, 10-18 parts of radix saposhnikoviae, 9-15 parts of myrrh, 6-12 parts of incised notopterygium, 5-11 parts of gypsum, 7-13 parts of Chinese asystasiella herb, 10-15 parts of herb of hairyfruit violet, 20-40 parts of carbomer, 14-18 parts of a substrate, 0.02-0.04 parts of a fibroblast growth factor, 2-4 parts of vitamin E, 1.0-1.4 parts of ethyl p-hydroxybenzoate as well as proper amounts of glycerol and triethanolamine. The gel prepared by the invention has functions of healing sore and relieving swelling, stopping bleeding and relieving pain, promoting wound healing and the like; the gel is good in biocompatibility, good in absorptivity, non-irritant to skin and good in antibacterial performance, and the gel is non-adhesive to a wound surface and is capable of relieving hyperplastic scars.

The invention discloses a nutrition beverage which takes sowthistle-leaf ixeris and natural fruits as raw materials. The weight ratio of sowthistle leaf ixeris juice, natural fruits juice and drinking water contained in the beverage is 1:0.5-50:0.5-50. The preparation method of the beverage comprises the following steps: the cleaned impurity-free sowthistle leaf ixeris and the cleaned and sliced natural fruits are weighed according to the mixture ratio and placed into a container, then added with clean water with the temperature of 80-100 DEG C according to the mixture ratio and naturally soaked in the clean water for 30-90 minutes, and directly extruded to obtain the beverage. The beverage keeps the natural flavor of the sowthistle leaf ixeris and the fruits, has unique and plentiful taste, and combines various pharmacological efficacies of the sowthistle leaf ixeris such as clearing heat and detoxifying, cooling blood and promoting blood circulation, reducing blood lipid, and protecting heart and blood vessels with trophism of various vitamins contained in the natural fruits, thus the beverage is a novel health beverage.

The invention discloses traditional Chinese medicine for treating spasmodic contraction of internal anal sphincter. The traditional Chinese medicine is composed of Chinese medicinal herbs including Rhodobryum roseum, Semen boitae, Polygala tenuifolia, Dens draconis, Jasminum grandiflorum, dung beetle, Stellaria dichotoma, manystem stonecrop leaf, Pteris multifida poir, Ixeris denticulata, root of common butterbush, hooked spikemoss, delavay raspberry herb, Galinsoga parviflora, Herba achyranthes asperae, Mentha crispata, Herba schizonepetae, Radix saposhnikoviae, Semen sinapis and Equisetum hiemale. The Chinese medicinal herbs which are pure natural are used as raw materials, so that the traditional Chinese medicine treats both symptoms and root causes, has exact treatment effect and is free of toxic and side effect and less prone to causing recurrence.

The invention belongs to technical the field of medicine and relates to the extraction of flavone and phenolic acid compounds from a medicinal material ixeris sonchifolia through a metal ion chelation process. A method for extracting and purifying flavones and phenolic acids in a medicinal material ixeris sonchifolia through metal ion chelation is characterized by comprising the following steps: (1) extraction; (2) solvent recovery and moisture removal; (3) dissolution in an organic solvent and filtering; (4) metal ion chelation; and (5) filtering and drying to obtain the product. The feature that flavones and phenolic acids often have o-diphenol hydroxyl or adjacent hydroxyl and carbonyl structures and can be chelated with metal ions is conducive to the chelation reaction in a certain alkalinity range, and the chelate can be precipitated in the organic solvent and separated out. The extraction technology of ixeris sonchifolia flavones is simplified, the extraction period is shortened, the technology is simple and easy to understand, and the production cost can be reduced; and moreover, the product has stable quality, loose property and good fluidity and facilitates further preparation processing.