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49 results about "Silver preparation" patented technology

Water-soluble nano silver preparation method based on waste keratin degradation products

The invention relates to a water-soluble nano silver preparation method based on waste keratin degradation products. The waste keratin degradation products are preprocessed, the waste keratin degradation products and distilled water are then put into a reaction kettle, and after thermal degradation is conducted on the waste keratin degradation products and the distilled water, a keratin solution is obtained; keratin polypeptide powder prepared after the keratin solution is purified and concentrated is used for preparing a keratin polypeptide aqueous solution, and the keratin polypeptide aqueous solution is mixed with a silver compound solution to prepare the water-soluble nano silver of different particle sizes under different temperature and pH value conditions. When the preparation method is compared with the prior art, the method that polypeptide chain sections obtained from the situation that the waste keratin materials are degraded through overheated water serve as a biological template to prepare nano materials is put forward for the first time. Water-soluble nano silver particles prepared through the method have good dispersity and good stability, and the particle sizes of the water-soluble nano silver particles can be controlled through changing of parameters; meanwhile, the whole process of the water-soluble nano silver particles is simple and easy to operate and capable of being directly applied to fields such as biological medicine because any chemical reagent and other hazardous substances do not participate in the preparation process.
Owner:DONGHUA UNIV

A kind of polymer surface protection monodisperse nano-silver particle and preparation method

The invention discloses a polymer surface protection monodisperse nano silver particle. A monodisperse ball-shaped efficient anti-agglomeration nano silver preparation is prepared in situ through a synthetic high polymer stabilizing additive containing sulfydryl under the effect of a mixed solvent by the action of silver nitrate and a reducing agent, and the grain size of the preparation is about 10 nanometers. The nano silver particle provided by the invention has outstanding dispersion, and the product of the invention can be used as a medical material for treating burns and scalds, and a material for treating skin infection of trauma patients and preventing and treating incision infection after skin and surgical operation incision. The nano silver particle has the excellent properties of broad-spectrum antibiotic property, long-acting property, kill drug resistance and the like.
Owner:翔瑞(泉州)纳米科技有限公司

Method for reclaiming silver and copper in silver-copper alloy scrap

The invention provides a method for recycling silver and copper in silver and copper alloy scrap, relating to a method for the wet recycling of the silver and copper in the silver and copper alloy scrap. The method is characterized in that the recycling process comprises the steps that the silver and copper alloy is firstly dissolved by using nitric acid, the solution is heated, evaporated and condensed to obtain silver nitrate and copper nitrate crystal; heating is continued to obtain a copper oxide mixture with decomposed silver nitrate and copper nitrate, water is slowly added into the mixture to cause the silver nitrate in the mixture to be dissolved, solid copper oxide and silver nitrate solution are separated out by filtration, and finally, a silver nitrate solution electro-deposition tank is added to directly carry out electro-deposition to prepare electro-deposited silver. Compared with the traditional method, the method of the invention eliminates the processes of chloridized silver deposition and copper separation, and hydrazine hydrate reduction silver-preparation, thus effectively reducing the reagent consumption and the silver-recycling cost. Acid-containing solution generated in the electro-deposition process can be circularly used for silver and copper alloy dissolving without emission. The method of the invention can separate and recycle silver and copper, with high efficiency, low cost and simplicity, and has high electro-deposited silver quality.
Owner:WESTERN METAL MATERIAL

Nano silver preparation process

The invention provides a nano silver preparation process, which is characterized by comprising the following steps: A. dissolving silver salt and a protective agent into a water soluble solvent or an alcohol solvent; B. adjusting the pH value into a needed range; C. adding a reducer to the obtained mixed solution, and heating and stirring for reacting for 20-30 minutes; and D. finally obtaining golden yellow nano silver solution. Compared with the prior art, the nano silver obtained by the preparation process of the invention is degradable, nontoxic and harmless to people and livestock, environmental friendly and soluble in water and most of organic matters totally, wherein, the particle size of the obtained nano silver product is less than 10nm and the complete reaction rate of silver ions is more than 99.99%. The nano silver preparation process has the advantages of simplicity, simple manufacturing equipment, low cost, food-grade raw materials and no any emissions and environmental pollution in the whole preparation course.
Owner:余运洋

System and method for in-situ conditioning of emitter electrode with silver

Cleaning and / or conditioning electrode surfaces can provide significant performance and operational benefits in EHD devices. In particular, conditioning of emitter electrode surfaces with silver (Ag), silver compositions or silver preparations applied in situ at successive times throughout the operating lifetime of an EHD air mover has been found to significantly reduce ozone production. Structures and techniques are described for in situ conditioning electrode surfaces and, in particular, emitter electrode surfaces of an EHD device such as an air mover or precipitator, with a conditioning material that includes silver.
Owner:PANASONIC PRECISION DEVICES

Chitosan oligosaccharide derivative and nano-silver preparation method

InactiveCN103182516AClear formation processConfirmation of basic optical characteristicsSilver preparationCHITOSAN OLIGOSACCHARIDE
The invention discloses a chitosan oligosaccharide derivative and a nano-silver preparation method. The nano-silver preparation method comprises the following steps of: (1) synthesizing chitosan oligosaccharide Schiff base S-COS; (2) synthesizing chitosan oligosaccharide phosphonate S-COS-P; and (3) preparing the nano-silver by reducing the chitosan oligosaccharide derivative. A method for synthesizing the chitosan oligosaccharide derivative by taking chitosan oligosaccharide as a raw material under the condition of microwave radiation is explored, and the structure of the chitosan oligosaccharide derivative is characterized, the optimum reaction conditions of the chitosan oligosaccharide derivative are explored, and simultaneously, the nano-silver is prepared by reducing the synthesized chitosan oligosaccharide derivative; and the nano-silver preparation method is preliminarily explored, and the structure of the nano-silver is characterized; and the preliminary conclusion of nano-silver preparation is obtained.
Owner:HENAN AGRICULTURAL UNIVERSITY

Functionalized graphene oxide supported nano-silver preparation method

The present invention discloses a functionalized graphene oxide supported nano-silver preparation method, and relates to a sterilization technique, wherein the functionalized graphene oxide supported nano-silver is preferably amino-modified polyethylene glycol functionalized graphene oxide supported nano-silver, and the modification component is amino-modified polyethylene glycol functionalized graphene oxide. Preferably the method comprises: preparing graphene oxide, preparing amino-modified polyethylene glycol modified graphene oxide, and finally preparing nano-silver respectively with particle sizes of 10 nm, 30 nm and 50 nm. According to the present invention, the functionalized graphene oxide supported nano-silver with different particle sizes are prepared and are used for the antibacterial field, and the particle size of the functionalized graphene oxide supported nano-silver having the optimal antibacterial effect is found through the antibacterial effect comparison.
Owner:FENGHUA YUCHUANG PROD DESIGN

Simple method for preparing nano silver from bacterial fermentation solution

The invention discloses a simple method for preparing nano silver from a bacterial fermentation solution. The method comprises the steps of inoculating staphylococcus aureus or enterococcus faecalis to a Mueller-Hinton culture medium, implementing shake cultivation for 12-72 hours at 25-37 DEG C, separating the thallus from bacterium suspension, reserving the bacterium suspension, adding a silver nitrate solution to the bacterium suspension so that silver ion concentration is 0.5-10mM, implementing shake cultivation for 5-72 hours at 25-37 DEG C, carrying out ultrasonic treatment, filtering the solution after the ultrasonic treatment, and reserving filtrate to obtain a nano silver solution. The method, which is used for preparing nano silver particles through the bacterial fermentation solution, is simple and easy, strong in operability and low in cost, and is free from toxic and harmful substances to the environment, thus being a simple and environment-friendly nano silver preparation technology.
Owner:GUANGDONG INST OF MICROBIOLOGY GUANGDONG DETECTION CENT OF MICROBIOLOGY

Method for preparing nano-silver from nanocellulose hydrogel

The invention discloses a method for preparing nano-silver from nanocellulose hydrogel, and belongs to the field of nano-silver preparation. The method comprises the steps that nano-hydrogel is prepared from nano-bamboo fiber, the hydrogel is soaked in a silver salt solution, silver ions are adsorbed through the internal network structure of the hydrogel and rich groups contained in the hydrogel, the hydrogel adsorbing the silver ions is put into a reducing agent to be soaked to generate nano-silver, and then impurity removing through separation and spray drying are performed to obtain nano-silver powder. The nano-silver prepared through the method is uniform in particle size, high in purity and good in dispersity, the prepared hydrogel is good in polymerization degree, and therefore the nano-silver powder of the small size can be obtained; in addition, the preparation conditions are easy to control, the cost is low, no surfactant needs to be added, and pollution to the environment is reduced.
Owner:CHANGZHOU DAAO NEW MATERIAL TECH CO LTD

Amphiphilic nano-silver preparation method based on polyurethane stabilizer

The invention relates to inorganic metal nano materials preparation, in particular to an amphiphilic nano-silver preparation method based on the reverse miniemulsion technology of a polyurethane stabilizer. The grain size of novel prepared amphiphilic nano-silver can range from 5 nanometers to 100 nanometers, and regulation and control can be achieved through easy control over reaction conditions such as reactant concentration and ultrasonic emulsification power; the amphiphilic nano-silver can be prepared by regulating and controlling the composition of the polyurethane stabilizer and has good dispersity and dispersion stability in a nonpolar solvent system like methylbenzene and polar solvent like water. A polyurethane stabilizer synthetic method is simple, the technology is controllable, the synthesis raw materials are easy to obtain and harmless, and industrial production is easy. The prepared amphiphilic nano-silver can be used as a function nano additive to be applied to various polymer systems, and the polymer materials have the functions of antibacterial property, electrical conductivity, photocatalytic property and the like.
Owner:RUNTAI CHEM TAIXING CO LTD

Method for preparing antibacterial plant tissue culture medium

The invention discloses a method for preparing an antibacterial plant tissue culture medium. According to the invention, a green pollution-free and low-cost nano-silver preparation method is adopted, which comprises the following steps of reducing a silver nitrate solution with D-glucose or galactose as a reducing agent in an aqueous solution by virtue of a liquid-phase chemical reduction method at 15-25 DEG C, and adding the obtained nano-silver sol into a culture medium, adding sucrose as a carbon source and an energy material and testing the resistance to bacteria in air of the nano-silver sol. The green pollution-free and low-cost nano-silver preparation method disclosed by the invention is simple and easily operated, the prepared nano-silver sol has the characteristics of uniform and moderate particle size and uniform dispersion. The nano-silver sol disclosed by the invention has good compatibility with the culture medium system. The culture medium in which the nano-silver sol is added has a good antibacterial effect.
Owner:ANKANG UNIV

Flower-like silver preparation method adopting gallic acid as structure-directing agent

The invention belongs to the technical field of nanometer material preparation, and particularly relates to a flower-like silver preparation method adopting gallic acid as a structure-directing agent.Under an ice-water bath, a silver nitrate water solution and a protective agent polyvinylpyrrolidone solution are added into ultra-pure water, magnetic stirring is performed, a structure-directing agent gallic acid solution is added into the system, continuous stirring is performed, a reducing agent ascorbic acid solution is rapidly injected into the system, a reaction is performed, after the reaction is finished, a reaction solution is taken out, and ultra-pure water is used for centrifugal cleaning to obtain flower-like silver particles. The prepared flower-like silver is of the complete and clear multi-level structure, the specific area is large, and the performance and the application field of silver nanoparticles are greatly enlarged.
Owner:ZHONGBEI UNIV

Liquid nano silver preparation method

The present disclosure relates to a liquid nano silver preparation method. The method comprises the following steps of 1, adding a stabilizer to a silver nitrate solution at room temperature and magnetic stirring; 2, stirring the mixture and adding an ascorbic acid solution, specifically, the molar ratio of silver nitrate to ascorbic acid is controlled to range from 1:4 to 1:7; 3, adding a sodiumhydroxide solution to control the pH value of a system to range from 7.6 to 8.0; and 4, stirring the mixture to obtain a liquid nano silver product. The liquid nano silver prepared by the method has an excellent antibacterial effect, and especially has an antibacterial effect against bacillus subtilis, and the antibacterial rate is almost 100%; the liquid nano silver can also inhibit the growth ofaspergillus niger, the inhibition rate is 90%, and the effective antibacterial time can be up to 30 days; the preparation method is simple and easy to implement, and conforms to the green chemistry concept.
Owner:BEIJING GUANGHE BIOTECH CO LTD

System and method for in-situ conditioning of emitter electrode with silver

InactiveUS8804296B2Significant performance and operational benefitReduce ozone productionWave amplification devicesElectrographic process apparatusSilver preparationPolymer chemistry
Cleaning and / or conditioning electrode surfaces can provide significant performance and operational benefits in EHD devices. In particular, conditioning of emitter electrode surfaces with silver (Ag), silver compositions or silver preparations applied in situ at successive times throughout the operating lifetime of an EHD air mover has been found to significantly reduce ozone production. Structures and techniques are described for in situ conditioning electrode surfaces and, in particular, emitter electrode surfaces of an EHD device such as an air mover or precipitator, with a conditioning material that includes silver.
Owner:PANASONIC PRECISION DEVICES

Nano-silver preparation for inhibiting mould Gra04 growth and preparation method thereof

The invention discloses a nano-silver preparation for inhibiting mould Gra04 growth and a preparation method thereof. The particle size of nano-silver in the nano-silver preparation is 10-40 nm; and the concentration of the nano-silver is 4.04*10-5 mol / L-16.16*10-5 mol / L. The preparation method comprises the following steps: firstly, NaOH water solution is added in AgNO3 water solution for stirring; supernatant is removed; then, dilute ammonia solution is added in obtained Ag2O precipitation for stirring; finally, PVP is added in obtained mixed liquid for stirring, is positioned in an photochemical reaction instrument for reacting and centrifugating; and the obtained precipitation is the nano-silver preparation.
Owner:NANJING UNIV OF POSTS & TELECOMM

Indoor air purifier of pure plant extracts

The invention discloses an indoor air purifier of pure plant extracts. The indoor air purifier contains natural pure plant extracts and ingredients and is prepared from the following raw materials: the natural pure plant extracts comprise 20-26 parts of eleocharis tuberose peel, 3-6 parts of gleditsia sinensis, 5-8 parts of green tea and 2-5 parts of licorice; and the ingredients comprise 1.2-1.5parts of zingiberone, 0.3-0.8 part of zingiberol, 0.1-0.3 part of plant essence, 0.2-1.2 parts of phellandrene, 0.9-1.2 parts of geraniol and additives. The nanometer Ag-carrying antibacterial agent silver preparation has good antibacterial performance; eleocharis tuberose peel, gleditsia sinensis, green tea, licorice and other natural plants can undergo complexation or absorption, adsorption andother complex actions with gases of thermal spring so as to achieve the purpose of purifying and refreshing the air; green tea also has bactericidal effect; a modified bentonite formaldehyde adsorbentcan have the effect of purifying formaldehyde; and zingiberone, zingiberol, plant essence, phellandrene and geraniol can react with odor molecules after being mixed so as to achieve the purpose of deodorization.
Owner:安徽桧元素生物科技有限公司

Simple method for preparing nano-silver based on plumeria rubra extracting solution

The invention discloses a simple method for preparing nano-silver based on a plumeria rubra extracting solution. A plumeria rubra ethanol extracting solution is mixed with a silver ion solution to react to generate the nano-silver. The plumeria rubra extracting solution is used for reducing silver ions to prepare the elementary substance nano-silver. The method can prepare nano-silver particles with the particle size of 1-57nm. According to the method, the plumeria rubra extracting solution is used for preparing the nano-silver particles, and the preparation method is simple, easy to implement, high in operability and low in cost. The plumeria rubra extracting solution serves as a reducing agent and a stabilizing agent at the same time, other chemical components do not need to be added in the reaction process, and a large number of nano-silver particles are prepared within a short time. The method is a simple and environmental-friendly nano-silver preparation method.
Owner:GUANGDONG INST OF MICROBIOLOGY GUANGDONG DETECTION CENT OF MICROBIOLOGY

Preparation method of nano-silver particle coated by novel macromolecule protective agent

A preparation method of a nano-silver particle coated by a novel macromolecule protective agent belongs to the technical field of manufacture of printing electronic materials. The steps comprise that a) a solution of the macromolecule protective agent with a certain temperature, a certain concentration and a certain pH value is prepared; b) a silver ammonia solution and a reductant solution are added into the macromolecule protective agent solution; c) the mixed solution is stirred, the pH value of the mixed solution is monitored in a real time, and the pH value of the mixed solution is kept to exceed 7 by adding a pH modifier; and the nano-silver particle can be prepared through a chemical reaction. In comparison with the prior art, the preparation method of the nano-silver particle coated by the novel macromolecule protective agent provided by the invention has the beneficial effect that acrylic-based resin with a multi-carbonyl structure is taken as the protective agent for the nano-silver preparation in an alkaline environment, wherein no research report has been proposed domestically; and because of outstanding aging resistance (such as the resistance to corrosion of acids, weak alkalis and salts) and adhesive force of the acrylic-based resin, the prepared nano-silver particle can guarantee requirements in applications for the adhesive force and the aging resistance without addition of other types of resin.
Owner:青岛纳印新材料科技有限公司

Nano-silver preparation method

The invention relates to a nano-silver preparation method which comprises the following steps: preparing 1-100 g / L of a silver nitrate methanol or ethanol solution, and then slowly adding an artemisinin-based drug for uniformly stirring; then putting the obtained mixture under an ultraviolet lamp for 5-60 minutes' illumination, so as to obtain a nano-silver colloidal solution, wherein the wave length and the power of the ultraviolet lamp are 365 nm and 50 W respectively; and then rinsing with ethanol as well as performing centrifugation and drying treatment, so as to obtain nano-silver. According to the nano-silver preparation method provided by the invention, artemisinin-based drugs are adopted as reducing agents and protecting agents of nano-silver; the nano-silver preparation method has the characteristics of being simple in process, wide in raw material source, mild in reaction, environmentally friendly and the like; and the prepared nano-silver has double effects of bacteria resistance and malaria resistance.
Owner:苏州巨联环保有限公司

Method for preparing nano-silver with different particle sizes by using surfactant

The invention relates to a method for preparing nano-silver with different particle sizes by using a surfactant. The method is characterized by comprising the following three steps of: (1) slowly dripping a surfactant solution into a silver nitrate solution with a certain concentration within 30-60 min to prepare a solution a; (2) dissolving a sufficient amount of a reducing agent and a surfactant in water to obtain a solution b, a concentration of the surfactant in the solution b being the same as that of the surfactant in the solution a, slowly dripping the solution b into the solution a within 60-150 min to obtain a solution c, and (3) cooling the solution c to room temperature, and adjusting the pH value of the solution to 3.0-9.5 by using a pH regulator to complete the preparation of the nano-silver, wherein stirring is needed during dripping, and the temperature is 20-50 DEG C. According to the method, controllability of the particle sizes in the nano-silver preparation process can be achieved according to the type and use quantity of the surfactant, the particle size of the prepared nano-silver ranges from 20.6 nm to 129.5 nm, and the prepared nano-silver has good compatibility with anion, cation and nonionic materials. The method is simple in preparation process operation, mild in reaction condition, wide in raw material source and high in practicability.
Owner:广东省江门市质量计量监督检测所 +1

A Simple Method for Preparation of Nano Silver Using Bacterial Fermentation Broth

The invention discloses a simple method for preparing nano silver from a bacterial fermentation solution. The method comprises the steps of inoculating staphylococcus aureus or enterococcus faecalis to a Mueller-Hinton culture medium, implementing shake cultivation for 12-72 hours at 25-37 DEG C, separating the thallus from bacterium suspension, reserving the bacterium suspension, adding a silver nitrate solution to the bacterium suspension so that silver ion concentration is 0.5-10mM, implementing shake cultivation for 5-72 hours at 25-37 DEG C, carrying out ultrasonic treatment, filtering the solution after the ultrasonic treatment, and reserving filtrate to obtain a nano silver solution. The method, which is used for preparing nano silver particles through the bacterial fermentation solution, is simple and easy, strong in operability and low in cost, and is free from toxic and harmful substances to the environment, thus being a simple and environment-friendly nano silver preparation technology.
Owner:GUANGDONG INST OF MICROBIOLOGY GUANGDONG DETECTION CENT OF MICROBIOLOGY

Preparation method of self-supporting nanometer porous silver electrode

The invention provides a nanometer porous silver preparation method, which comprises: immersing a solid material at least containing silver on the surface into a liquid electrolytic solution containing transition metal ion and a metal chloride, wherein the solid material is used as precursor; promoting the silver surface to spontaneously form silver chloride by using the transition metal cation through a micro battery reaction; and carrying out electrical reduction to form nanometer porous silver. The invention further provides a preparation method of a self-supporting nanometer porous silverelectrode, wherein the self-supporting nanometer porous silver electrode is prepared by using a silver electrode as a precursor through the method. Compared with the nanometer porous silver in the prior art, the nanometer porous silver of the present invention has the following characteristics that the silver surface spontaneously form the silver chloride by using the transition metal cation through the micro battery reaction, and the electrical reduction is performed to form the nanometer porous silver, such that the oxygen reduction activity is significantly improved compared with the original silver electrode. Compared with the method in the prior art, the method of the present invention eliminates the energy consumption process for applying voltage to the silver electrode to form AgClso as to reduce the energy consumption, and further has advantages of simpleness, strong controllability and the like.
Owner:QINGDAO UNIV OF SCI & TECH

Method for preparing nano-silver based on red spinach extracting solution

The invention discloses a method for preparing nano-silver based on a red spinach extracting solution. The method is characterized by mixing the red spinach ethanol extracting solution with the silver ion solution, and reacting to generate the nano-silver. According to the method, the red spinach extracting solution is used for reducing silver ions to prepare the simple substance nano-silver. The nano-silver particles with the particle size of 1-30 nm can be prepared according to the method provided by the invention. The nano-silver particles are prepared from the red spinach extracting solution, the preparation method is simple and easy to implement, high in operability and low in cost, the red spinach extracting solution serves as a reducing agent and a stabilizing agent at the same time, other chemical components do not need to be added in the reaction process, a large number of nano-silver particles are prepared within a short time, the method is a simple and environment-friendly nano-silver preparation method, and the prepared nano-silver solution has a high antibacterial effect.
Owner:GUANGDONG INST OF MICROBIOLOGY GUANGDONG DETECTION CENT OF MICROBIOLOGY

Acrylic fiber conductive filament and chemical silvering preparation method

The invention discloses an acrylic fiber conductive filament and a chemical silvering preparation method. The method takes acrylic fiber filament as a matrix, and fully uses an acrylic fiber filamentbark-like surface structure and -CN electronegativity, the acrylic fiber filament is subjected to degreasing, coarsening and activation, and is subjected to pressurization, heating and dipping in an enclosed alkaline silver ammonium solution for chemical plating, and a white silver simple substance is formed at the surface of acrylic fiber, so that the filament conductive processing is carried out. The prepared acrylic fiber conductive filament has the advantages of easy control, good conductivity, strong fiber affinity capability, lasting conductive characteristic, excellent sterilization deodorizing shielding property, and good acid and alkali resistance.
Owner:CHANGSHU XIANGYING SPECIAL FIBER

Nano-silver dispersion liquid and preparation method thereof

The invention provides a nano-silver dispersion liquid and a preparation method thereof, and belongs to the technical field of nano-silver preparation. The preparation method comprises the following steps of mixing gamma-aminopropyltriethoxysilane, polyvinylpyrrolidone, sodium dodecyl sulfate, silver nitrate and water, and performing chelation to obtain a chelating dispersion liquid, wherein the time for putting the gamma-aminopropyltriethoxysilane in air before mixing is less than 5 minutes; and dropwise adding a sodium borohydride solution into the chelating dispersion liquid, and performingredox reaction to obtain the nano-silver dispersion liquid. The nano-silver dispersion liquid prepared by the method disclosed by the invention is small in particle size of nano-silver and good in dispersity.
Owner:QINGDAO TECHNOLOGICAL UNIVERSITY

Color developing system for responding to rot smell of meat through color change, and preparation method and application thereof

The invention discloses a nano-silver color developing system for responding to a rot smell of meat through color change, and a preparation method and an application thereof, and belongs to the fieldof food monitoring. According to the color developing system, an Arabic gum powder solution is added into a silver nitrate solution and the solutions are stirred uniformly; then a reaction is carriedout under a high-temperature and high-pressure condition; and after the reaction is ended, filtering is carried out to obtain the Arabic gum powder-nano-silver color developing system. Compared with atraditional nano-silver preparation method, the preparation method has the following advantages: the preparation method of the Arabic gum powder-nano-silver color developing system which follows "green chemistry" shows the advantages of safety, non-toxicity, environmental friendliness and the like, and greatly reduces the toxic effect generated by the traditional preparation method. By selectinga food-grade safe medium, the potential toxicity generated for the environment and organisms is reduced. Meanwhile, certain harm to the environment caused by toxic substances generated in a synthesisprocess is avoided.
Owner:NANJING AGRICULTURAL UNIVERSITY

High-wear-resistance composite material for preparing porcelain teeth and preparation method of high-wear-resistance composite material

The invention relates to the technical field of medical materials, in particular to a high-wear-resistance composite material for preparing porcelain teeth and a preparation method of the high-wear-resistance composite material. The high-wear-resistance composite material is prepared from the following raw materials in parts by weight: 20 to 30 parts of metal oxygen compound, 8 to 15 parts of metal nitride whisker, 18 to 30 parts of titanium dioxide, 10 to 30 parts of silicon dioxide, 30 to 40 parts of zirconium dioxide, 5 to 8 parts of silver preparation, 120 to 160 parts of 80% ethanol and 50 to 70 parts of deionized water. The titanium dioxide modified by the titanate coupling agent is added, so that the corrosive wear of the artificial saliva to the porcelain tooth material can be slowed down to a certain extent, and the life cycle of the porcelain tooth is prolonged; the silane coupling agent modified zirconium dioxide is added, so that the mechanical property of the porcelain tooth material can be enhanced, and the porcelain tooth material can meet the use requirements of people in daily life.
Owner:中山市邦特生物科技有限公司

Externally-applied nano silver preparation and preparation method thereof

The invention discloses an externally-applied nano silver preparation and a preparation method thereof. The preparation comprises lanonol, cetanol, lecithin, sorbitan, Tween-80, dimethyl p-aminobenzene methyl caprylin and mineral oil which form an oil phase, glycerol and deionized water which form a water phase, as well as nano sliver particle, cerous nitrate, acetic acid, chitosan and sodium polyacrylate. According to the method disclosed by the invention, the water-phase material and the oil-phase material flow into an emulsification neutralization tank for emulsification after being heated, and nano silver master rubber, cerium preliminary liquor and chitosan are added, and finally, the externally-applied nano sliver preparation is prepared. The preparation disclosed by the invention has a bacteriostatic effect and a sterilization effect, and particularly has very obvious effects for intractable pseudomonas aeruginosa and staphylococcus aureus. Besides, the externally-applied nano silver preparation has good permeability so as to be applied to a deep wound part, has good astringency to accelerate healing of a wound surface, is free from irritability and has an effect of promoting epithelial cells to grow.
Owner:SHANGHAI UNIV

Preparation method of nano-silver cube

The invention discloses a preparation method of a nano-silver cube, belonging to the technical field of three-dimensional nano-silver preparation. The method of the invention comprises the steps of using a mixed solution of ethylene glycol and glycerin as a solvent and a reducing agent, FeS2 as a controlling agent, and polyvinylpyrrolidone (PVP) and tetraethylammonium bromide as a surfactant, andusing silver nitrate to provide a silver source, so as to rapidly synthesize the nano-silver cube with assistance of microwaves. The method of the invention has the advantages that the raw material iseasy to obtain, the process is simple, the equipment is easy to obtain, the process is easy to operate, the production time is short, the efficiency is high, and the size of the product nano-silver cube is uniform.
Owner:KUNMING UNIV OF SCI & TECH

Preparation method of kelp-shaped silver structure

The invention belongs to the technical field of nano-silver preparation, and discloses a preparation method of a kelp-shaped nano-silver structure. The preparation method comprises the following stepsthat S1, a mixed solution of hydrofluoric acid, silver nitrate and SDS is prepared; S2, a cleaned silicon wafer is soaked in the mixed solution prepared in the S1 to react for a period of time; and S3, after the reaction, the silicon wafer is cleaned up, and blow-drying is carried out to obtain the kelp-shaped nano-silver structure, wherein in the S1, the concentration of the hydrofluoric acid inthe mixed solution is 10<-6> M-10 M, the concentration of the silver nitrate in the mixed solution is 10<-6> M-1 M, and the concentration of the SDS in the mixed solution is 10<-6> M-1 M. The methodis simple to operate, low in cost and simple and convenient in process, and facilitates the preparation of a novel kelp-shaped nano-silver structure.
Owner:INT ACAD OF OPTOELECTRONICS AT ZHAOQING SOUTH CHINA NORMAL UNIV
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