The invention discloses a multi-element high-activity element
coating for forming a self-repairing Al2O3 protective layer in a non-
oxygen-control
lead bismuth alloy and a preparation method of the multi-element high-activity element
coating. The method comprises the following steps: 1, carrying out pre-
grinding and
polishing treatment on the surface of a matrix, and then carrying out ultrasonic cleaning and
drying; (2) embedding in
powder containing Al and Cr, and sealing; 3, placing in a
heating furnace, and filling protective gas for heating and heat preservation; 4, soaking in liquid lead-
bismuth alloy; and 5, cleaning and
drying. According to the method, high-activity elements Al and Cr are introduced by adopting a
powder burying and heating method, an Al2O3
oxide layer is formed by combining a liquid lead-
bismuth alloy soaking method to serve as a
diffusion barrier, dissolved
oxygen and Pb-Bi are prevented from invading into a
crystal boundary, alloy elements are prevented from being dissolved and leached into LBE, the effect of isolating
liquid metal from a
metal matrix is achieved, oxidation
corrosion is prevented from being further generated, and the service life of the LBE is prolonged. The
corrosion protection method is suitable for the fields of nuclear
corrosion,
liquid metal corrosion, corrosion protection of
nuclear reactor structure materials and the like.