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Combination including calcium conjugated linoleic acid and producing method thereof

A technology of calcium conjugated linoleate and conjugated linoleic acid, which is applied in the field of high-purity calcium conjugated linoleate products and its preparation, can solve the problem of unsatisfactory properties, unsatisfactory color, and no specific report on the milk production of dairy cows to achieve good physical properties, improve purity, and increase milk production

Active Publication Date: 2007-09-12
INNOBIO CORP LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

According to the content disclosed in the patent, the composition can effectively reduce the fat content in milk and increase the content of CLA, but there is no specific report on the effect of the composition on the milk production of cows
This patent also discloses the preparation method of the above-mentioned composition containing conjugated calcium linoleate. However, this method is used to produce in the same equipment, and various components in the raw vegetable oil are brought into the product, and the obtained product is conjugated The percentage composition of calcium linoleate is lower than 80% (disclosed content of embodiment); And saturated fatty acid in the product, as the content of palmitic acid and stearic acid etc. is higher, conjugated calcium linoleate accounts for total fatty acid calcium The mass percentage is lower than 85%; secondly, the obtained product is a block solid, although it can meet the requirements as a feed additive after crushing, its properties, color, etc. are not very satisfactory

Method used

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  • Combination including calcium conjugated linoleic acid and producing method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] Add 4.8 liters of methanol and 81 grams of potassium hydroxide to 11 liters of sunflower oil, react at 35°C for 2 hours, separate out the glycerol after cooling down, then carry out molecular distillation at 6 Pa and 160°C to obtain 90% methyl linoleate. Take 7.5 liters of methyl linoleate, add 4 liters of methanol, 1.7 kg of potassium hydroxide, and react at 150° C. for 5 hours.

[0036] In a 50-liter reactor, add 16 liters of water and 14 liters of methanol to 7.5 kg of potassium salt rich in conjugated linoleic acid. After fully stirring and dissolving, slowly add concentrated hydrochloric acid to adjust the pH to 9-10, and slowly add 3.9 kg of 35% calcium chloride aqueous solution was added dropwise while stirring, the kettle temperature was controlled at about 30° C., reacted for 3 hours, suction filtered, and the filter cake was vacuum-dried to obtain the product.

[0037] components

Mass percentage

CLA-Ca

Other Fatty Acid Calcium

moi...

Embodiment 2

[0044] Add 250 milliliters of methanol, 6 grams of caustic soda to 550 milliliters of safflower oil, react for 2.5 hours at 40° C., separate glycerin after cooling, then carry out molecular distillation at 2 Pa and 140° C. to obtain 90% methyl linoleate. Take 150 milliliters of methyl ester, add 120 milliliters of methanol, 25-30 grams of caustic soda, and react at 155° C. for 4.5 hours under normal pressure.

[0045] In a 2-liter glass reactor, add 300 ml of water and 200 ml of ethanol to 145.3 g of sodium salt rich in conjugated linoleic acid. After fully stirring and dissolving, slowly add concentrated hydrochloric acid to adjust the pH to 9-10, slowly Add 75 milliliters of 40% calcium chloride aqueous solution dropwise, stir while adding dropwise, the kettle temperature is controlled at about 40°C, react for 2 hours, filter with suction, and obtain the product after the filter cake is vacuum-dried.

[0046] components

Mass percentage

CLA-Ca

Calcium...

Embodiment 3

[0053]In 2.5 liters of Suaeda salsa seed oil, add 1.2 liters of methanol, 20 grams of KOH, react at 62°C for 2.5 hours, separate out glycerol after cooling; carry out molecular distillation at 6Pa, under the condition of 150°C to obtain 85% methyl linoleate; Add 150 ml of methyl ester, add 120 ml of methanol, 30 g of caustic soda, and react for 4.5 hours under normal pressure at 155°C.

[0054] In a 2-liter glass reactor, add 300 ml of water and 200 ml of ethanol to 145.3 g of sodium salt rich in conjugated linoleic acid. After fully stirring and dissolving, slowly add concentrated hydrochloric acid to adjust the pH to 9-10, slowly Add 75 milliliters of 40% calcium chloride aqueous solution dropwise, stir while adding dropwise, the kettle temperature is controlled at about 40°C, react for 2 hours, filter with suction, and obtain the product after the filter cake is vacuum-dried.

[0055] components

Mass percentage

CLA-Ca

Calcium other fatty acids

...

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PUM

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Abstract

The present invention discloses one kind of composition containing calcium conjugate linoleate for increasing the milk output of milk cow and its preparation process. The composition is prepared with vegetable oil as material, and through ester exchange reaction, molecular distillation, saponification, isomerization and metathetical reaction. It consists of alphatic calcium, water and impurity salt; and the alphatic calcium includes calcium conjugate linoleate accounting for 82-90 wt% of the composition, calcium palmitate, calcium stearate, calcium oleate and calcium linoleate accounting for 8-15 wt% of the composition. It has high calcium conjugate linoleate content, controllable content of other kinds of alphatic calcium and excellent physical character. It is used in raising milk cow to raise milk output obviously.

Description

technical field [0001] The invention relates to a composition containing calcium conjugated linoleate and a preparation method thereof, in particular to a high-purity calcium conjugated linoleate product for increasing milk production of dairy cows and a preparation method thereof. Background technique [0002] Conjugated Linoleic Acid (CLA) belongs to polyunsaturated fatty acid and is a group of isomers of linoleic acid. Adding conjugated linoleic acid in the feed can significantly increase the CLA content in milk and reduce the saturated fatty acid in milk. In order to avoid the destruction of conjugated linoleic acid when it passes through the rumen of cows, the calcium salt of conjugated linoleic acid is often used as a feed additive. Studies have shown that the addition of calcium conjugated linoleate (CLA-Ca) can increase the content of CLA in milk and reduce the content of saturated fatty acids in milk. However, there are few studies on the effect of CLA-Ca on milk ...

Claims

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Application Information

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IPC IPC(8): A23K1/16A23K1/00A61K31/201A61P15/14A61P15/00A23K20/10A23K20/24A23K40/00A23K50/10
Inventor 吴文忠刘明徐维锋刘强
Owner INNOBIO CORP LTD
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