Resin composition capable of polymerizing
A polymeric resin and composition technology, applied in coatings, instruments, organic chemistry, etc., can solve the problems of reduced transmittance of coating films or patterns, high sublimation, and pollution inside baking ovens, etc.
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Embodiment 1
[0244] The following components were mixed: 169 parts (55 parts in terms of solid content) of the resin solution (A) containing the resin (i) obtained in Synthesis Example 1, 45 parts of dipentaerythritol hexaacrylate (B), 4 parts 2,2'-bis(2-chlorophenyl)-4,4',5,5'-tetraphenylbiimidazole (C), 0.5 part 2-(2-naphthoylmethylene)- 3-Methylbenzothiazoline (C-1), 4 parts of pentaerythritol tetrathiopropionate (T), 56 parts of propylene glycol monomethyl ether acetate (D) and 40 parts of 3-ethoxyethylpropionate acid ester to obtain polymerizable resin composition 1.
[0245]
[0246]
[0247] A 2-inch glass substrate (#1737; manufactured by Corning) was washed sequentially with a neutral detergent, water, and alcohol, and then dried. On this glass substrate, the polymerizable resin composition 1 was spin-coated and 200 mJ / cm 2 (405 nm) exposure, developed and washed with water so that the film thickness after post-baking was 3.0 μm, and then pre-baked at 100° C. for 3 minutes...
Embodiment 2
[0260] Polymerizable resin composition 2 was obtained in the same manner as polymerizable resin composition 1 to provide the formulations shown in Table 1, and evaluated. The results are described in Table 2.
Embodiment 3
[0262] Polymerizable resin composition 3 was obtained in the same manner as in Example 1 to provide the formulations shown in Table 1, and evaluated. The results are described in Table 2.
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