Use of human recombination hepatic stimulator substance for reinforcing anti-apoptosis of liver cancer cell and application thereof
A technology of liver-stimulating factor and human recombination, which is used in medical preparations containing active ingredients, anti-tumor drugs, drug combinations, etc.
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Embodiment 1
[0027] Example 1: Construction of vectors expressing human recombinant liver-stimulating factor
[0028] Using the mouse HSS gene probe, human HSS was amplified by RT-PCR. After DNA sequence analysis, a gene named hHSS containing an open reading frame (open reading frame, ORF) was obtained, which was inserted into the pcDNA3.1 plasmid (Invitrogen ) to construct pcDNA3.1-hHSS at the corresponding site.
Embodiment 2
[0029] Example 2: Cell culture and transfection
[0030] The BEL-7402 liver cancer cell line was cultured in DEME medium containing 15% fetal bovine serum at 37°C, 5% CO 2 cultivated under conditions.
[0031] Transfection: transfection and screening with hHSS gene by 1×10 4 Inoculate BEL-7402 liver cancer cells at a cell density of / ml in three 25cm 2 In culture flasks, cells were cultured in DMEM medium. When the cell density reaches 3×10 5 / ml (60-80% cell confluency), remove the culture medium, with no Ca 2+ , Mg 2+ Dulbecco's PBS (pH 7.4) washed 3 times to eliminate the influence of residual serum. Serum-free DMEM medium (containing insulin 10 μg / ml) was added. The hHSS gene transfection was carried out the next day. Prepare four 1.5ml sterile Eppendorf tubes, two corresponding to the marks. Take 5 μg each of pcDNA3.1-hHSS and pcDNA3.1, put them into two Eppendorf tubes, and make 0.1 μg / μl with HBS (HEPES-buffer saline). Another 60 μl of DOTAP (N-[2,3-Dioleoylox...
Embodiment 3
[0033] Example 3: Physicochemical properties and structural stability of recombinant hHSS
[0034] Under conditions suitable for recombinant protein expression, the monoclonal cell lines obtained in Example 2 expressing human recombinant liver stimulating factor and empty vector were expressed. The human recombinant liver-stimulating factor protein was recovered and purified, and its physical and chemical properties and structural stability were detected by synchronous fluorescence spectroscopy and circular dichroism spectroscopy.
[0035] see figure 1 , the test results showed that the purified recombinant hHSS was a homodimeric protein with a molecular weight of 31kD and an isoelectric point of 4.5.
[0036] see figure 2 3. Through the research of recombinant hHSS by simultaneous fluorescence spectroscopy and circular dichroism spectroscopy, it was found that the secondary structure of hHSS is very stable, and has strong acid and alkali resistance and high temperature res...
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