PDP fluorescent powder pulp for spraying and preparation thereof
A technology for phosphors and pastes, applied in luminescent materials, chemical instruments and methods, etc., can solve the problems of uneven particle size distribution, interruption of spraying process, difficult adhesion, etc., achieve uniform particle size distribution, avoid nozzle blockage, The effect of improving the hanging performance
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Embodiment 1
[0041] Preparation process I:
[0042] Put 5.5% (mass percentage, the same below) anti-settling agent polyamide wax and 15.5% ethyl acetate into a container made of non-metallic material or lined with non-metallic material, turn on high-speed stirring and set the stirring speed to 2000~ 2500rpm, use a disc-shaped stirrer coated with non-metallic material on the surface to stir and disperse the anti-sedimentation agent polyamide wax and ethyl acetate suspension for 5-10 minutes, until the suspension becomes a paste mixture.
[0043] Take another container made of non-metallic material or lined with non-metallic material, put in 6% nitrocellulose and 39% cyclohexanone, turn on the stirring device and stir at a low speed until the nitrocellulose is completely dissolved, during which the stirring speed is 300-400rpm , Stirring time 10 ~ 15min. After the nitrocellulose is completely dissolved, add the above pasty mixture, increase the stirring speed, and carry out high-speed stirr...
Embodiment 2
[0048] Preparation process I:
[0049] Put 7% anti-settling agent polyethylene wax and 17% ethyl acetate into a container made of non-metallic material or lined with non-metallic material, turn on high-speed stirring and set the stirring speed at 3000-3500rpm, use surface coated with Stir and disperse the anti-sedimentation agent polyethylene wax and ethyl acetate suspension with a non-metallic disc stirrer for 5-20 minutes until the suspension becomes a paste mixture.
[0050] Take another container made of non-metallic material or lined with non-metallic material, put in 5% ethyl cellulose and 36% ethyl lactate, turn on the stirring device and stir at a low speed until the ethyl cellulose is completely dissolved, during which the stirring speed is 250 ~350rpm, stirring time 15~20min. After the ethyl cellulose is completely dissolved, add the above pasty mixture, increase the stirring speed, stir at a speed not lower than 1000rpm, stir and disperse for 70-80min, until the pa...
Embodiment 3
[0055] Preparation process I:
[0056] Put 6% anti-sedimentation agent polypropylene wax and 15% butyl acetate into a container made of non-metallic material or lined with non-metallic material, turn on high-speed stirring and set the stirring speed at 2500-3000rpm, use surface coated with Stir and disperse the anti-settling agent polypropylene wax and butyl acetate suspension with a non-metallic disc stirrer for 10-15 minutes until the suspension becomes a paste mixture.
[0057] Take another container made of non-metallic material or lined with non-metallic material, put in 6.5% butyl cellulose and 35% ethyl benzoate, turn on the stirring device and stir at a low speed until the butyl cellulose is completely dissolved, during which the stirring speed is 350~400rpm, stirring time 25~30min. After the butyl cellulose is completely dissolved, add the above paste mixture, increase the stirring speed, and stir at a speed not lower than 1000rpm, stir and disperse for 30-40min, unt...
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