Method for extracting vanadium by stone coal and sulfuric acid wet pile oxidation conversion at normal temperature and pressure
A technology of atmospheric pressure and sulfuric acid, applied in the field of vanadium extraction, can solve the problems of high equipment requirements, environmental pollution, low leaching rate, etc., and achieve the effects of less investment in equipment, wide application range, and high recovery rate
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Embodiment 1
[0022] (1) dry-grinding the stone coal primary ore containing 0.98% vanadium mass percentage into stone coal powder with a particle size of about 1mm; (2) adding according to the mass ratio of stone coal powder: sulfuric acid: water=100:12:8 Industrial sulfuric acid and water, stirred evenly, under normal temperature and pressure, wet heap for 9 days, with a height of about 4 meters; (3) under normal temperature and pressure, add water according to the ratio of solid-liquid weight ratio of 1:1, stir and leach 70 minutes, adjust the pH value to 2.5, filter to remove residue, and obtain a blue vanadyl sulfate solution. The vanadium leaching rate is 80%.
Embodiment 2
[0024] (1) dry-grinding the stone coal primary ore containing 0.98% vanadium mass percentage into stone coal powder with a particle size of about 1mm; (2) adding according to the mass ratio of stone coal powder: sulfuric acid: water=100:15:8 Industrial sulfuric acid and water, stirred evenly, under normal temperature and pressure, wet heap for 9 days, with a height of about 4.5 meters; (3) under normal temperature and pressure, add water according to the ratio of solid-liquid weight ratio of 1:1, stir and leaching 80 minutes, adjust the pH value to 2.5, filter to remove residue, and obtain a blue vanadyl sulfate solution. Vanadium leaching rate is 78%.
Embodiment 3
[0026] (1) dry-grinding the stone coal primary ore containing 0.98% vanadium mass percentage into stone coal powder with a particle size of about 1mm; (2) adding according to the mass ratio of stone coal powder: sulfuric acid: water=100:20:7 Industrial sulfuric acid and water, stirred evenly, under normal temperature and pressure, wet heap for 7 days, with a height of about 5 meters; (3) under normal temperature and pressure, add water according to the ratio of solid-liquid weight ratio of 1:1.2, stir and leach 50 Minutes, adjust the pH value to 2.6, filter to remove residue, and obtain a blue vanadyl sulfate solution. Vanadium leaching rate is 91%.
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