Aligning agent for liquid crystal and liquid crystal display element
A technology of liquid crystal aligning agent and polymer, applied in liquid crystal materials, chemical instruments and methods, optics, etc., can solve problems such as damage to liquid crystal orientation, and achieve the effect of good coating and excellent film thickness uniformity
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[0138] Synthesis example 1
[0139] 109 g (0.50 mol) of pyromellitic dianhydride as tetracarboxylic dianhydride, 98 g (0.50 mol) of 1,2,3,4-cyclobutane tetracarboxylic dianhydride, and 4 as a diamine compound 200g (1.0 mol) of 4-diaminodiphenyl ether was dissolved in a mixed solvent made of 244g of N-methyl-2-pyrrolidone and 2200g of γ-butyrolactone. After reacting at 40°C for 3 hours, an additional 1220g of γ- Butyrolactone, about 4070 g of a solution containing 10% by weight of polyamic acid (A-1) was obtained. The solution viscosity of this solution was 200 mPa·s.
Example Embodiment
[0140] Synthesis Example 2
[0141] Combine 98 g (0.50 mol) of 1,2,3,4-cyclobutane tetracarboxylic dianhydride as tetracarboxylic dianhydride, 109 g (0.50 mol) of pyromellitic dianhydride, and 4, as a diamine compound, 198g (1.0 mol) of 4'-diaminodiphenylmethane was dissolved in a mixed solvent made of 243g N-methyl-2-pyrrolidone and 2190g γ-butyrolactone. After reacting at 40°C for 3 hours, an additional 1210g was added γ-butyrolactone, about 4050 g of a solution containing 10% by weight of polyamic acid (A-2) was obtained. The solution viscosity of this solution was 125 mPa·s.
Example Embodiment
[0142] Synthesis Example 3
[0143] 196 g (1.0 mol) of 1,2,3,4-cyclobutane tetracarboxylic dianhydride as tetracarboxylic dianhydride and 200 g (1.0 mol) of 4,4'-diaminodiphenyl ether as a diamine compound ) Was dissolved in a mixed solvent made of 238g N-methyl-2-pyrrolidone and 2130g γ-butyrolactone, and after reacting at 40°C for 4 hours, 1190g γ-butyrolactone was added to obtain about 3960g containing 10% by weight poly A solution of amic acid (A-3). The solution viscosity of this solution was 210 mPa·s.
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