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Preparation method of high-purity chlorine dioxide gas

A chlorine dioxide and gas technology, applied in chlorine oxide, gasification substances and other directions, can solve the problems of simple gasification technology, low automatic control level, and many equipment, etc., achieve scientific gasification technology, realize safe disinfection and gasification Reasonable effect of craftsmanship

Active Publication Date: 2011-04-06
广州净度环境科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, for the original air sterilizer, although great progress has been made, there are still some defects, mainly, the gasification process is cumbersome, the equipment is many, not compact, the gasification technology is simple, the equipment structure is unreasonable, and the gasification The purity of chlorine dioxide gas is low, chlorine gas is produced, the utilization rate of the liquid medicine is low, and the level of automatic control is low. Especially in the implementation of air disinfection, there are certain unsafe factors, especially in the case of people, people will feel uncomfortable. I feel that under the same disinfection effect, compared with the new technology, it has poor safety, large volume and high raw material consumption
At present, there is no method and special device for preparing high-purity chlorine dioxide gas by using the automatic control gas distribution positive pressure gasification technology in China

Method used

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  • Preparation method of high-purity chlorine dioxide gas
  • Preparation method of high-purity chlorine dioxide gas
  • Preparation method of high-purity chlorine dioxide gas

Examples

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Effect test

Embodiment 1

[0022] Using the gas distribution positive pressure gasification technology, the stable chlorine dioxide solution and dilute hydrochloric acid are added to the gasifier 10 in a molar ratio of 1:3.5-4.4 for reaction, and at the same time, the gas-liquid ratio is controlled to be 58.3:1, and the compressed air The lower part and the upper part in the gasifier are continuously transported through the gas distributor 8, and the gas volume ratio is controlled to be 0.2: 1 (v / v), and the gasification and generation of high-purity chlorine dioxide gas with a purity of 100% is mixed with compressed air, and passed The gas conveyor 4 will quickly take it out of the gasifier, control the gas volume ratio to 0.27:1 (v / v), and transport it to about 63m together with another introduced compressed air 3 Air disinfection is carried out in an observation room of a hospital emergency center, and the transportation distance is about 32m. After 60 minutes of disinfection, take samples according ...

Embodiment 2

[0025] Using the gas distribution positive pressure gasification technology, the stable chlorine dioxide solution and hydrochloric acid are added to the gasifier 10 in a molar ratio of 1:3.5-4.4 for reaction, and at the same time, the gas-liquid ratio is controlled to be 95.5:1, and the compressed air 6 The lower part and the upper part in the gasifier are continuously transported through the gas distributor 8, and the gas volume ratio is controlled to be 0.27: 1, and the gasification generation purity is that 100% high-purity chlorine dioxide gas is mixed with compressed air, and the gas is mixed with the compressed air through the gas conveyor 4. It is quickly taken out of the gasifier, the gas volume ratio is controlled to be 0.3:1, and it is transported together with another compressed air 6 to about 40m 3 Air disinfection is carried out in the debridement room of a hospital emergency center, and the delivery distance is about 25m. After 60 minutes of disinfection, take sa...

Embodiment 3

[0028] Using the gas distribution positive pressure gasification technology, the stable chlorine dioxide solution and hydrochloric acid are added to the gasifier 10 in a molar ratio of 1:3.5-4.4 for reaction, and at the same time, the gas-liquid ratio is controlled to 46.7:1, and the compressed air 6 The lower part and the upper part in the gasifier are continuously transported through the gas distributor 8, and the gas volume ratio is controlled to be 0.15: 1, and the gasification generation purity is that 100% high-purity chlorine dioxide gas is mixed with compressed air, and the gas is mixed with the compressed air through the gas conveyor 4. It is quickly taken out of the gasifier, the gas volume ratio is controlled to be 0.26:1, and it is transported to about 180m together with another introduced compressed air 3 Air disinfection is carried out in the emergency room of a hospital emergency center, and the transportation distance is about 45m. After 60 minutes of disinfect...

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Abstract

The invention discloses a preparation method and a special device of high-purity chlorine dioxide gas. The preparation method comprises the following steps of: conveying compressed air into a gasifier (10) through a gas distributor (8) and controlling the distribution ratio of the compressed air at the lower part and the upper part of the gasifier (10); and carrying out gasification reaction between stable chlorine dioxide solution and diluted hydrochloric acid in the gasifier (10) to obtain the high-purity chlorine dioxide gas. The method takes the stable chlorine dioxide solution as a disinfectant and adopts the special device to prepare the high-purity chlorine dioxide gas, the gas purity is improved by 100 percent from current 80 percent, and simultaneously, the medicine liquid utilization ratio is improved, the emission is reduced, and the yield of the product is also remarkably improved. The method can convey the produced high-purity chlorine dioxide gas into a required space rapidly, timely and quantitatively for air sterilization, thereby not only improving the security and realizing the safety sterilization, but also being capable of achieving better disinfection and sterilization effect.

Description

technical field [0001] The invention relates to a method for preparing high-purity chlorine dioxide gas, and also relates to a special device for realizing the preparation method, which belongs to the field of preparation of disinfectants. Background technique [0002] In recent years, because chlorine dioxide has the advantages of rapid sterilization, good sterilization effect, no residue, and no side effects, it has been more and more recognized by people. At present, it has gradually expanded from a wide range of water disinfection fields to air disinfection fields. [0003] In the field of air disinfection using chlorine dioxide, it has now developed from the initial simple use methods such as spraying, spraying, or natural volatilization to chlorine dioxide air disinfection machines. However, for the original air sterilizer, although great progress has been made, there are still some defects, mainly, the gasification process is cumbersome, the equipment is many, not com...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B11/02A61L9/015A61L101/06
Inventor 赖立克陈祥衡梁乃棉赖亮丁勇林徐建平
Owner 广州净度环境科技股份有限公司
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