Conductive polymer foams, method of manufacture, and uses thereof
A technology of polymers and foams, applied in conductive materials dispersed in non-conductive inorganic materials, transportation and packaging, thin material processing, etc., can solve problems such as difficulty in obtaining conductive foams
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Embodiment 1
[0144] Nickel microspheres and nickel-coated ceramic microspheres were evaluated as conductive fillers in polysiloxane foams. Polysiloxane (Dow Corning Silicone 8137 and NUSIL 6033 from NusilTechnology LLC), filler microspheres and polysiloxane cure inhibitor (1-octyn-3-ol from Aldrich Chemical Co.) Mixed in a speed mixer, cast on PET film at controlled thickness and placed in an oven exposed to an adjustable magnetic field. Typically, the chemically foamed and cured foam has a thickness of 70 to 80 mils (1778 to 2032 microns).
[0145] The results in Table 1 show that no electrical conductivity was observed in the thick cured foam layer even under strong magnetic fields up to 1200 Gauss.
[0146] Table 1
[0147] Test serial number
1
2
3
4
5
6
7
magnetic field, gauss
250
250
1000
1000
1200
1200
1200
Cast thickness, mil
10
20
20
20
20
...
Embodiment 2
[0151] Table 2 shows the results of additional testing with 100% nickel microspheres. Formulations were cast to a thickness of 18 to 40 mils (457 to 1016 microns) to prepare foam samples.
[0152] Test serial number
[0153] In the tests shown in Table 2, the formation of filler columns was observed; however, the foam was not conductive. Tests 1 to 3 were cast without a top carrier, resulting in poor foam quality. Analysis of Tests 4-13 indicated that the cured foam had a thickness of 40 to 120 mils (1016 to 3038 microns) and had two or more cells (z-direction) spanning the thickness of the foam.
Embodiment 3
[0155] Thinner foams were prepared using 100% nickel spheres or silver coated nickel spheres, both with and without top support, as indicated. Chill the premix in the freezer. Results are shown in Table 3A.
[0156] Test serial number
1a
1b
2a
2b
3a
3b
4a
4b
magnetic field, gauss
500
500
250
250
250
250
250
250
Cast thickness, mil
5
5
5
5
5
5
10
10
Oven temperature, ℃
55
55
55
55
50
50
50
50
Oven residence time, minutes
5
5
5
5
5
5
5
5
top carrier
none
Have
none
Have
none
Have
none
Have
base
PET
PET
PET
PET
PET
PET
PET
PET
Si formulation, A / B, g
33 / 3.3
33 / 3.3
33 / 3.3
33 / 3.3
33 / 3.3
...
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