Method for protecting substrates and removing contaminants from such substrates
A technology for contaminants and substrates, applied in chemical instruments and methods, cleaning methods and utensils, preparation of detergent mixture compositions, etc., can solve problems such as troublesome marking
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Embodiment 1
[0052] A jacketed 1 liter reactor, equipped with a thermocouple, condenser, and stirrer, was charged with 667.2 g of distilled water, 4.2 g of Byk-028, and 4.6 g of 46% by weight sodium hydroxide. The resulting aqueous composition was stirred until the salt had dissolved, then 169.6 g of Celvol 523 were added. The mixture was heated to 85°C for 30 minutes and then cooled to 65°C. 48.3 g of 95% ethanol was added, followed by dropwise addition of 25.4 g of BYK-420. The resulting formulation was then stirred at 65°C for one hour. A premix of 1.7 g Dowicil 75 and 121.1 g distilled water was added slowly with vigorous stirring. The mixture was then filtered to generate Formulation A. Formulation A had a Brookfield viscosity (3 rpm, 25°C, L4 spindle) of 59250 centipoise (cP) and a pH = 7.74.
[0053] 200.0 g of Formulation A neat was added to 800.0 g of deionized (DI) water with moderate agitation and stirred for 20 minutes to generate Formulation B.
Embodiment 2
[0055] A jacketed 1 liter reactor, equipped with a thermocouple, condenser, and stirrer, was charged with 667.2 g of distilled water, 4.2 g of Byk-028, and 4.6 g of 46% by weight sodium hydroxide. The resulting aqueous composition was stirred until the salt had dissolved, then 169.6 g of the water soluble polymer Celvol 508 was added. The mixture was heated to 85°C for 30 minutes and then cooled to 65°C. 48.3 g of 95% ethanol were added dropwise, followed by 25.4 g of BYK-420. The resulting formulation was then stirred at 65°C for one hour. A premix of 1.7 g of Dowicil 75 and 121.1 g of distilled water was added slowly with vigorous stirring. The mixture was then filtered to generate Formulation C. Formulation C had a Brookfield viscosity (3 rpm, 25°C, L4 spindle) of 23740 centipoise and pH = 7.28.
[0056] 100.0 g of Formulation C neat was added to 400.0 g of deionized (DI) water with moderate agitation and stirred for 20 minutes to generate Formulation D.
[0057] Tests...
Embodiment 3
[0059] Formulation E was formed by mixing 96.0 g of neat Formulation B with 4.0 g of BYK 333 (a product from Chemie under the name Polyether Modified Dimethicone Copolymer) with moderate agitation for 10 minutes.
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