Coating composition for antireflection, antireflection film and method for preparing the same
An anti-reflection film, composition technology, applied in anti-reflection coatings, nanotechnology for materials and surface science, coatings, etc., can solve the problems of difficult to obtain wear resistance, poor wear resistance, resolution deterioration, etc. , to achieve the effect of reducing production cost, improving processing efficiency, excellent wear resistance and low refraction characteristics
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[0095] The method for preparing an anti-reflection film according to the present invention includes the following steps:
[0096] a) Preparation of the above coating composition for anti-reflection;
[0097] b) coating the coating composition on the substrate to form a coating;
[0098] c) drying the coating to separate the low-refractive material and the high-refractive material; and
[0099] d) Curing the dried coating.
[0100] In step b), the substrate can be glass, plastic sheet and film, and its thickness is not limited. Examples of the plastic film may include cellulose triacetate film, norbornene cycloolefin polymer film, polyester film, polymethacrylate film, and polycarbonate film, but are not limited thereto.
[0101] In step b), the method for coating the coating composition can be, for example, bar coating, two-roll or three-roll reverse coating, gravure coating, die coating, microgravure coating There are various methods of comma coating and comma coating. The coating met...
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[0111] Best practice
[0112] In the following, preferred embodiments are provided for a better understanding of the present invention. However, these examples are for illustrative purposes only, and are not intended to limit the present invention by these examples.
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[0131] Example 1
[0132] 30 parts by weight of low-refraction-thermosetting material A and 70 parts by weight of high-refraction-UV curing material E were uniformly mixed to prepare a coating composition for antireflection.
[0133] A wire bar (No. 5) was used to coat the obtained composition on a cellulose triacetate film having a thickness of 80 μm. Dry the film in an oven at 60℃ for 2 minutes, and irradiate 1J / cm 2 Cured with a dose of UV, followed by thermal curing in an oven at 120°C for 1 day. The final coating thickness is 1μm, and the cross section is observed under a transmission electron microscope, which is shown in figure 1 in.
[0134] Reference figure 1 It was found that a high-refractive material layer and a low-refractive material layer were formed in a layer structure on the substrate. Compared with a single layer structure, when the layer structure is formed of materials having different refractive indexes, more effective reflectivity can be obtained.
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