Ultraviolet curing composition and preparation method thereof and pattern preparation method
A technology of ultraviolet light and composition, which is applied in the photographic process of patterned surface, photomechanical equipment, and photosensitive materials used in optomechanical equipment, etc., can solve problems such as substrate deformation, avoid substrate deformation, improve The effect of product quality
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[0023] In the specific preparation method of the ultraviolet curable composition of the present invention, the polyurethane acrylic resin, active monomer, photoinitiator and epoxy acrylic resin can be mixed once or step by step. In a preferred situation, first mix the photoinitiator with part of the active monomer to fully dissolve the photoinitiator to obtain a photoinitiator slurry; then mix the polyurethane acrylic resin with another part of the active monomer evenly to obtain a resin component slurry; then Mix the photoinitiator slurry with the resin component slurry evenly. The above mixing is usually carried out at room temperature, and it can also be slightly heated to 30-60°C to speed up the mixing.
[0024] Similarly, in the process of preparing the above-mentioned UV curable composition, a defoamer and a leveling agent may also be added. When the UV-curable composition to be prepared contains a defoamer and a leveling agent, the order of adding the defoamer and the ...
Embodiment 1
[0050] This example is used to illustrate the UV-curable composition disclosed in the present invention and its preparation method.
[0051] With 48g polyurethane acrylic resin (UV-3000B produced by Japan Synthetic Chemical Company, the weight average molecular weight is 18000), 38g dipentaerythritol hexaacrylate (SR399 produced by Sartomer), 2gIrgacure651 (produced by Ciba, Switzerland) and 12 rings An oxyacrylic acid resin (CNUVE151 produced by Sartomer Company) was added into a high-speed mixer, stirred at a speed of 1000 rad / min for 10 min, and filtered to obtain a UV-curable composition S1.
Embodiment 2
[0053] This example is used to illustrate the UV-curable composition disclosed in the present invention and its preparation method.
[0054] With 54g polyurethane acrylic resin (the UV-3000B that Nippon Synthetic Chemical Company produces, weight-average molecular weight is 20000), 32g hexanediol diacrylate (BASF company production), 2.8g Irgacure184 (Swiss Ciba company production) and 11.2g bis Phenol A epoxy resin (CN111 produced by Sartomer, USA) was added into a high-speed mixer, stirred at a speed of 1000 rad / min for 10 min, and filtered to obtain UV-curable composition S2.
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