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Energy-saving distillation method and device through differential pressure column section heat integration in rectification column sequences

A rectification tower and heat integration technology, applied in the field of rectification, can solve the problems of high operating cost, large diameter of the tower body, large operating reflux, etc., and achieve the effect of saving operating costs, reducing total energy consumption, and small energy consumption.

Inactive Publication Date: 2011-02-09
TIANJIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] For the existing multi-component separation conventional distillation sequence such as figure 1 As shown, when separating difficult-to-separate systems, the number of theoretical plates required is large, resulting in a large height of the tower; the operating reflux ratio of the required tower is large, resulting in a large diameter of the tower body, and the reboiler at the bottom of the tower The required heat load and the condensation load required by the overhead condenser are larger, so the energy consumption of the tower is higher and the operating cost is also higher

Method used

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  • Energy-saving distillation method and device through differential pressure column section heat integration in rectification column sequences
  • Energy-saving distillation method and device through differential pressure column section heat integration in rectification column sequences
  • Energy-saving distillation method and device through differential pressure column section heat integration in rectification column sequences

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Embodiment 1

[0034] Embodiment one (methanol, ethanol, propanol system separation)

[0035] Situation 1: Methanol, ethanol, and propanol are separated, and the process described in the present invention is adopted. Feed rate 1000kg / h, feed composition: methyl alcohol, 33.3% (wt%), ethanol, 33.3% (wt%), propanol, 33.4% (wt%), feed heat state is bubble point feed. The number of theoretical plates in the distillation column of light components is 60, and the number of theoretical plates in the rectification column section and stripping column section of the light component refining column is 30 respectively. The operating pressure of the light-ends distillation tower and the light-ends refining tower rectification column section is 1.50 atm, and the operating pressure of the light-ends refining tower stripping column section is 0.58 atm. The output of the bottom product of the light component distillation tower is 335kg / h, and the purity of the extracted product is controlled above 99.5% (wt...

Embodiment 2

[0069] Embodiment two (2-methylpentane, n-hexane, cyclohexane system separation)

[0070] Situation 1: 2-methylpentane, n-hexane, and cyclohexane are separated, and the process described in the present invention is adopted. Feed amount 1000kg / h, feed composition: 2-methylpentane, 33.3% (wt%), n-hexane, 33.3% (wt%), hexanaphthene, 33.4% (wt%), feed heat condition Feed for bubble point. The number of theoretical plates in the distillation column of light components is 80, and the number of theoretical plates in the rectification column section and stripping column section of the light component refining column is 60 respectively. The operating pressure of the light-ends distillation tower and the light-ends refining tower rectification column section is 1.50 atm, and the operating pressure of the light-ends refining tower stripping column section is 0.58 atm. The output of the bottom product of the light component distillation tower is 335kg / h, and the purity of the extracted ...

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Abstract

The invention relates to an energy-saving rectification device and method through differential pressure column section heat integration in rectification column sequences. The device comprises a light component boil-up column, a light component refining column rectification column section, an auxiliary condenser, a return tank, a flash tank, a light component refining column stripper section, an auxiliary reboiler and a main reboiler, wherein the light component boil-up column is used for pressurizing the light component refining column rectification column section; a top saturated vapor outlet pipe of the light component refining column rectification column section is connected to the heat media inlet of the main reboiler; the heat media outlet of the main reboiler is connected to the inlet of the auxiliary condenser; a bottom liquid outlet pipe is connected to the inlet of the return tank; a bottom liquid outlet pipe of the light component refining column stripper section is connected to the cold media inlet of the auxiliary reboiler and the cold media inlet of the main reboiler respectively; and the cold media outlets of the auxiliary reboiler and the main reboiler are respectively connected to a reboiled vapor inlet pipe of the light component refining column stripper section. The invention realizes single-column heat integration and matched heat exchange in the rectification column sequences. The invention realizes minimum heat consumption of the single column through differential pressure column section heat integration, even ensures the cold and heat load to be perfectly matched and ensures zero consumption, thus greatly reducing energy consumption of the system and achieving the aims of energy saving and synergy.

Description

technical field [0001] The invention relates to the technical field of rectification and a rectification tower system, in particular to a heat-integrated energy-saving rectification device and method for differential pressure tower sections of a rectification tower sequence. Background technique [0002] Distillation is the most widely used industrial separation method in contemporary times, and has been widely used in chemical industry, petroleum, food, light industry and other industrial sectors. Although the development of science and technology, new separation technology has begun industrial application, but in a certain period of time, the dominance of rectification technology cannot be shaken. [0003] Distillation separation technology is mature and easy to industrialize, but the disadvantage is that it consumes a lot of energy. For traditional distillation and separation, the input energy consumption accounts for more than 40% of the total industrial energy consumpt...

Claims

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Application Information

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IPC IPC(8): B01D3/38B01D3/42
Inventor 袁希钢闫兵海刘春江罗祎青许良华曾爱武唐忠利
Owner TIANJIN UNIV
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