Energy-saving distillation method and device through differential pressure column section heat integration in rectification column sequences
A rectification tower and heat integration technology, applied in the field of rectification, can solve the problems of high operating cost, large diameter of the tower body, large operating reflux, etc., and achieve the effect of saving operating costs, reducing total energy consumption, and small energy consumption.
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Embodiment 1
[0034] Embodiment one (methanol, ethanol, propanol system separation)
[0035] Situation 1: Methanol, ethanol, and propanol are separated, and the process described in the present invention is adopted. Feed rate 1000kg / h, feed composition: methyl alcohol, 33.3% (wt%), ethanol, 33.3% (wt%), propanol, 33.4% (wt%), feed heat state is bubble point feed. The number of theoretical plates in the distillation column of light components is 60, and the number of theoretical plates in the rectification column section and stripping column section of the light component refining column is 30 respectively. The operating pressure of the light-ends distillation tower and the light-ends refining tower rectification column section is 1.50 atm, and the operating pressure of the light-ends refining tower stripping column section is 0.58 atm. The output of the bottom product of the light component distillation tower is 335kg / h, and the purity of the extracted product is controlled above 99.5% (wt...
Embodiment 2
[0069] Embodiment two (2-methylpentane, n-hexane, cyclohexane system separation)
[0070] Situation 1: 2-methylpentane, n-hexane, and cyclohexane are separated, and the process described in the present invention is adopted. Feed amount 1000kg / h, feed composition: 2-methylpentane, 33.3% (wt%), n-hexane, 33.3% (wt%), hexanaphthene, 33.4% (wt%), feed heat condition Feed for bubble point. The number of theoretical plates in the distillation column of light components is 80, and the number of theoretical plates in the rectification column section and stripping column section of the light component refining column is 60 respectively. The operating pressure of the light-ends distillation tower and the light-ends refining tower rectification column section is 1.50 atm, and the operating pressure of the light-ends refining tower stripping column section is 0.58 atm. The output of the bottom product of the light component distillation tower is 335kg / h, and the purity of the extracted ...
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