Method for processing low-temperature pyrolyzed coal tar

A technology of low-temperature coal tar and processing method, which is applied in the processing of tar, the processing of removing tar by water, and the processing of refining tar by chemical method, etc., can solve problems such as comprehensive utilization and waste of resources, achieve reasonable utilization, low cost, and solve The effect of difficult separation of oil and water

Inactive Publication Date: 2011-02-16
CHINA COAL RES INST
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Problems solved by technology

[0004] The early methods of low-temperature pyrolysis of coal tar mainly used processing methods such as centrifugal separation, atmospheric and vacuum distillation, solvent dilution precipitation and distillation coking. Because low-temperature coal tar contains a large amount of phenol (an important chemical raw material, Account for about 35% of total weight,), and existing these methods all can not extract phenol, cause the low-temperature coal tar that contains many precious compounds (as phenolic compound etc.) at present only as a kind of low price, even cheap Liquid fuels are sold in the market, which is a great waste of comprehensive utilization of resources

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  • Method for processing low-temperature pyrolyzed coal tar
  • Method for processing low-temperature pyrolyzed coal tar

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Embodiment Construction

[0013] This specific embodiment provides a processing method for low-temperature pyrolysis coal tar, which is mainly composed of five parts: preprocessing before processing, alkali extraction, crude phenate purification, crude phenol refining, and processing of the remaining part after alkali extraction. The technical scheme is clearly described, and will be described below in conjunction with the accompanying drawings of the description, such as figure 1 As shown, the method may specifically include:

[0014] In step 1, the low-temperature coal tar to be pyrolyzed is deslagged through a super centrifuge.

[0015] In order to obtain a higher extraction rate of crude phenoxide, the low-temperature coal tar to be pyrolyzed can be pre-deslagged first, and the coarse slag can be removed by a high-speed centrifuge to obtain the low-temperature coal tar to be pyrolyzed. Wherein said super centrifuge can select the centrifuge that rotating speed is 50000r / min.

[0016] In step 2, t...

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Abstract

The invention relates to a method for processing low-temperature pyrolyzed coal tar. The method comprises the following steps of: pressurizing and standing low-temperature coal tar to be pyrolyzed, dehydrating initially by changing surface tension, adding a demulsifying agent to form azeotropic water through light oil circulation and performing final dehydration; extracting crude phenate from the dehydrated low-temperature coal tar by alkaline washing; purifying the extracted crude phenate through oil-water mixed gas and decomposing through carbon dioxide so as to obtain crude phenol; and dehydrating the obtained crude phenol, deslagging and rectifying so as to obtain a target product. By the method, the phenol extraction rate of the low-temperature pyrolyzed coal tar is over 95 percent, the problem of difficult oil and water separation can be solved and the dehydration rate after processing is between 0.5 and 1 percent. The method is a processing method which has low cost and reasonably utilizes a low-temperature coal tar resource.

Description

technical field [0001] The invention relates to a low-temperature pyrolysis coal tar processing method, in particular to a low-temperature pyrolysis coal tar processing method in which phenol is first extracted and then distilled. Background technique [0002] According to the different pyrolysis temperature, coal tar can be divided into low-temperature coal tar and high-temperature coal tar. With the massive development of low-rank coal with abundant reserves in my country, the reasonable separation and processing of low-temperature coal tar has become an important issue in the field of pyrolysis coal tar. [0003] Due to the low pyrolysis temperature and a small amount of secondary pyrolysis, the composition characteristics and processing methods of low-temperature coal tar are obviously different from those of high-temperature coal tar. The content of phenolic compounds and saturated hydrocarbons is also higher than that of high-temperature coal tar, while the content of a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10C1/02C10C1/20C10C1/00
Inventor 曲思健商铁成裴贤丰王彬张飏赵奇孙会青鲁励
Owner CHINA COAL RES INST
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