Method for simultaneously measuring high-pressure gas adsorption capacity and adsorption swell capacity of coal petrography and measuring equipment

A technology of adsorption expansion and high-pressure gas, which is applied to the analysis of materials and instruments, and can solve the problems of difficulty in measuring adsorption amount and adsorption deformation, inability to measure at the same time, and no device and measurement method for measuring adsorption amount and adsorption deformation expansion.

Inactive Publication Date: 2011-02-16
SHANXI INST OF COAL CHEM CHINESE ACAD OF SCI
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  • Abstract
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  • Application Information

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Problems solved by technology

The test results show that the adsorption capacity of coal with the same degree of metamorphism varies within a certain range, and the adsorption capacity of coal in the same mine and the same coal seam can only reach a similar level.
[0007] The characteristics of the above measurement techniques and devices are that either they can only measure the amount of adsorption, or they can only measure the amount of deformation.
Among these measurement methods, powdered coal samples or lump coal samples are usually used as test samples for the adsorption capacity test, and lump coal samples are used for the adsorption expansion test. Since the adsorption capacity and adsorption expansion tests use different coal samples , and cannot simultaneously measure
As a result, the measured adsorption amount and adsorption expansion deformation cannot be well corresponded, and the measured adsorption amount and adsorption deformation are quite different from the actual values ​​of adsorption amount and adsorption deformation of coal rocks under in-situ conditions.
[0008] It is difficult to measure the adsorption amount and adsorption deformation simultaneously on a sample, so there are few reports on this work
At present, there is no related report on the device and measurement method for simultaneously measuring the adsorption capacity and adsorption deformation expansion on a sample.

Method used

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  • Method for simultaneously measuring high-pressure gas adsorption capacity and adsorption swell capacity of coal petrography and measuring equipment
  • Method for simultaneously measuring high-pressure gas adsorption capacity and adsorption swell capacity of coal petrography and measuring equipment
  • Method for simultaneously measuring high-pressure gas adsorption capacity and adsorption swell capacity of coal petrography and measuring equipment

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Experimental program
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Effect test

Embodiment 1

[0090] The measuring device is composed of a high-pressure test container 1, a high-pressure reference container 2, a displacement sensor 3, a first pressure transmitter 5, a second pressure transmitter 4, a constant temperature bath box 19 and a measurement control instrument 23. The four walls are equipped with semiconductor refrigeration chips 16, and the inside of the constant temperature box 19 is equipped with a heating pipe 8, a temperature measuring thermal resistance 9, a circulation pump 17, a high-voltage test container 1 and a high-voltage reference container 2; The cylinder body 11, ferrule 12, air inlet and air outlet are composed, and a gasket 14 is installed between the upper cylinder body 11 and the lower cylinder body 10, and the upper cylinder body 11 and the lower cylinder body 10 are connected and fixed by the ferrule 12, A displacement sensor 3 is installed on the top of the upper cylinder body 11, a gasket 34 is arranged between the displacement sensor 3 ...

Embodiment 2

[0123] Set the temperature at 65°C, and the high pressure test gas is CH 4 Under the condition of gas, all the other are with embodiment 1.

Embodiment 3

[0125] Set the temperature at 25°C, and the high pressure test gas is N 2 Under the condition of gas, all the other are with embodiment 1.

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Abstract

The invention provides a method for simultaneously measuring high-pressure gas absorption capacity and adsorption sell capacity of coal petrography and measuring equipment, which can simultaneously measure the adsorption capacity and adsorption swell capacity of the coal petrography in high-pressure gas at a pressure of 0-20MPa and a temperature of 0-80 DEG C. In the process of measurement, a measurement and control device is used for performing signal transformation and analog-to-digital conversion on electrical signals of a displacement sensor, a temperature-measuring hot resistor and a pressure transmitter; a computer is used for automatically receiving pressure, temperature and displacement signal data from the measurement and control device and recording and saving the received data; and a computer screen is used for displaying the pressure, temperature, adsorption capacity and swell capacity data timely in the process of measurement and the change law curves of the pressure, the temperature and the swell capacity with the change of time in real time. In the method of the invention, the measurement on the adsorption capacity and the adsorption swell capacity can be finished simultaneously, so that the method is simple and convenient and fast, and has the advantages of simple structure, reliable and safe high-pressure seal, easy operation, high measurement accuracy, high resistance to pressure and automatic measurement.

Description

technical field [0001] The invention belongs to a method and a measuring device for simultaneously measuring the adsorption amount and the adsorption expansion amount of high-pressure gas of coal rocks. Background technique [0002] Coal rock mass is a porous medium containing a large amount of adsorbed coalbed methane, and its mechanical properties have an important impact on coalbed methane mining. The pore characteristics, adsorption and desorption characteristics and geological control mechanism of coal and coal reservoirs have always been hot issues concerned by the coalbed methane and geological circles. The adsorption of coal is an important basis for evaluating the gas content and recoverability of coalbed methane. The understanding of the adsorption / desorption characteristics of coalbed methane has a profound impact on the evaluation of recoverable resources of coalbed methane and the numerical simulation of coal reservoir productivity. The kinetic model and mechan...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N7/04
Inventor 刘增厚杨建丽陈国青刘振宇李允梅刘平光
Owner SHANXI INST OF COAL CHEM CHINESE ACAD OF SCI
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