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Method for pulping cotton linter

A linter production and linters technology, which is applied in textiles, papermaking, and fiber raw material processing, can solve the problems of affecting the cooking quality, lowering the heating temperature, and not being able to remove linters grease and wax

Active Publication Date: 2011-04-20
合肥银山棉麻股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the domestic counterparts and relevant scientific research institutes have successively studied the method of adding hydrogen peroxide for cooking and bleaching when the cotton linters are cooking and feeding, because the heating temperature in the later stage of cooking is reduced, and the cooking quality is affected.
Since hydrogen peroxide can only bleach the surface of the fiber and cannot penetrate into the interior, and hydrogen peroxide cannot remove the oil and wax of cotton linters, it cannot effectively improve the reactivity of cotton pulp and cannot be used to make chemical fiber cotton pulp

Method used

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  • Method for pulping cotton linter
  • Method for pulping cotton linter
  • Method for pulping cotton linter

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] 1. Cooking

[0021] (1) Feeding

[0022] Drop into cotton linters and sodium hydroxide solution in 40 cubic meters of steaming balls, the absolute dry weight of feeding intake of cotton linters is 4500kg, the alkali consumption rate is 17% (NaOH quality / cotton linters absolute dry weight), sodium hydroxide solution The concentration of the sodium hydroxide solution is 50g / L, the temperature of the sodium hydroxide solution entering the ball (that is, the temperature of the sodium hydroxide solution before entering the ball): ≥90°C, the dosage of the sodium hydroxide solution: 15.3m 3 .

[0023] (2) heating up once

[0024] See image 3 Middle A-B section.

[0025] (3) A small release of steam

[0026] See image 3 Middle B-C section.

[0027] (4) Secondary heating

[0028] See image 3 Middle section C-D.

[0029] (5) Secondary small steam release

[0030] See image 3 Middle D-E section.

[0031] (6)Three heating up

[0032] See image 3 Middle E-F secti...

Embodiment 2

[0049] All the other are the same as embodiment 1, the difference is

[0050] 1. When cooking:

[0051] (9) Add hydrogen peroxide

[0052] The quality of hydrogen peroxide dilution is 6T, which contains 135kg of pure 100% H 2 o 2 .

[0053] When the pressure of the steam ball is less than 0.05MPa and the temperature is 105°C, add hydrogen peroxide, and after all the hydrogen peroxide diluent is added, perform the following operations at 80-90°C: stop the steam ball at the position where the steam is released, and turn it on. Steaming ball circulation pump, the liquid in the steaming ball is pumped out from the lower part of the steaming ball, and the steaming ball is injected from the upper part of the steaming ball to make the liquid in the steaming ball circulate internally for 20 minutes, then stop the internal circulation and start the steaming ball to rotate for 20 minutes. The total processing time from adding hydrogen peroxide to pouring is 60 minutes.

[0054] After...

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Abstract

The invention provides a method for pulping cotton linter, which can reduce COD (Chemical Oxygen Demand) in black liquor generated by stewing to be less than 8,000mg / L and simultaneously improve the reaction performance of cotton pulp. The method for pulping cotton linter comprises the stewing step, wherein the stewing step comprises the following concrete steps of: (1) mixing the cotton linter with sodium hydroxide solution and preserving the temperature at the stewing temperature; (2) releasing the steam; (3) adding hydrogen peroxide diluted solution when the gauge pressure is less than 0.05MPa, wherein the weight of H2O2 is 3-6 percent that of the cotton linter, and pouring materials treated at the temperature of 80-100DEG C. By using the invention, the stewing quality and bleaching of the stewing pulp can be ensured, and a large amount of organic matters in the black liquor can be oxygenolyzed and settled. Before washing materials, a sample is taken out from a washing pool and detected, wherein the fiber whiteness is more than 60 percent, the dust content is less than 0.9 percent, the iron content is less than 60ppm and the reaction performance is not more than 50s; meanwhile, the COD in the filtered black liquor is reduced to be less than 8,000mg / L from 100,000-160,000mg / L in the prior art.

Description

technical field [0001] The invention relates to a method for pulping cotton linters. Background technique [0002] In the field of chemical fiber and refined cotton production in China, cotton linter pulping includes the following steps: cooking, washing, beating, sand removal, bleaching, and pulping. The block diagram of the entire production process is as follows figure 1 shown. Among them, the cooking of cotton linters must go through ten procedures: feeding, first heating, first small steam release, second heating, second small steam release, third heating, heat preservation, large steam release, warming water, and feeding. Cooking achieves the purpose of heating up by introducing high-temperature water vapor into the steaming ball, and adopts the well-known small release of steam while heating up (see image 3 ) method to achieve the required temperature and gauge pressure during heat preservation. During cooking, cotton linters undergo saponification and emulsificat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21C5/00
Inventor 薛润林
Owner 合肥银山棉麻股份有限公司