Anode mixture for nonaqueous electrolyte secondary cell, anode for nonaqueous electrolyte secondary cell, and nonaqueous electrolyte secondary cell
A non-aqueous electrolyte and secondary battery technology, applied in the direction of non-aqueous electrolyte batteries, battery electrodes, circuits, etc., can solve the problem of insufficient peel strength of the current collector and the mixture layer, and achieve the effect of excellent peel strength
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Embodiment 1
[0146] 8 g of vinylidene fluoride polymer-(1) containing chlorine atoms and polar groups was uniformly dissolved in 92 g of N-methyl-2-pyrrolidone to obtain a binder solution.
[0147] Add 9.2g of MAG (manufactured by Hitachi Chemical Co., Ltd., artificial graphite, average particle size 20μm) and 4.61g of N-methyl-2-pyrrolidone for dilution to 10g of the resulting binder solution, and use defoaming stirring Taro (manufactured by Shinki ) Stir and mix to obtain a negative electrode mixture (1) for a non-aqueous electrolyte secondary battery.
[0148] Using a bar coater, the above-mentioned negative electrode mixture (1) for non-aqueous electrolyte secondary batteries was uniformly coated on a rolled copper foil with a thickness of 10 μm as a current collector so that the weight of the dried mixture layer was 150 g / m 2 In a gear oven (gear oven), dried at 110°C, heat treated at 130°C, pressurized at 40MPa, and the bulk density of the mixture layer is 1.7g / cm 3 The electrode (1). The...
Embodiment 2
[0150] 8 g of vinylidene fluoride polymer-(2) containing chlorine atoms and polar groups was uniformly dissolved in 92 g of N-methyl-2-pyrrolidone to obtain a binder solution.
[0151] Add 9.2g of MAG (manufactured by Hitachi Chemical Co., Ltd., artificial graphite, average particle size 20μm) and 4.61g of N-methyl-2-pyrrolidone for dilution to 10g of the resulting binder solution, and use defoaming stirring Taro (manufactured by Shinki ) Stir and mix to obtain a negative electrode mixture (2) for a non-aqueous electrolyte secondary battery.
[0152] Using a bar coater, the above-mentioned negative electrode mixture (2) for non-aqueous electrolyte secondary batteries was uniformly coated on a rolled copper foil with a thickness of 10 μm as a current collector so that the weight of the dried mixture layer was 150 g / m 2 , In a Geer aging thermostat, dried at 110°C, heat treated at 130°C, and pressurized at 40MPa to obtain a mixture layer with a bulk density of 1.7g / cm 3 The electrodes...
Embodiment 3
[0154] 8 g of vinylidene fluoride polymer-(3) containing chlorine atoms and polar groups was uniformly dissolved in 92 g of N-methyl-2-pyrrolidone to obtain a binder solution.
[0155] Add 9.2g of MAG (manufactured by Hitachi Chemical Co., Ltd., artificial graphite, average particle size 20μm) and 4.61g of N-methyl-2-pyrrolidone for dilution to 10g of the resulting binder solution, and use defoaming stirring Taro (manufactured by Shinki ) Stir and mix to obtain a negative electrode mixture (3) for a non-aqueous electrolyte secondary battery.
[0156] Using a bar coater, the above-mentioned negative electrode mixture for non-aqueous electrolyte secondary batteries (3) was uniformly coated on a rolled copper foil with a thickness of 10 μm as a current collector so that the weight of the dried mixture layer was 150 g / m 2 , In a Geer aging thermostat, dried at 110°C, heat treated at 130°C, and pressurized at 40MPa to obtain a mixture layer with a bulk density of 1.7g / cm 3 The electrodes...
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Abstract
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