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Preparation method of odontal restoration material

A tooth restoration and repair material technology, applied in dental preparations, dental prosthesis, dentistry, etc., can solve problems such as high cost, complex structure, and industrial production restrictions, and achieve excellent performance, simple raw material acquisition, and simple technical operation steps easy effect

Inactive Publication Date: 2012-11-28
TONGJI HOSPITAL ATTACHED TO TONGJI MEDICAL COLLEGE HUAZHONG SCI TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the complexity of the molecular structure of these organic substances, the cost of their preparation process is high, which limits the industrial production in batches.

Method used

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  • Preparation method of odontal restoration material
  • Preparation method of odontal restoration material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] 1) Take the caries-free premolars extracted for orthodontic treatment, remove the roots and enamel, and cut them into 2*2*1.5mm by using a high-speed turbine 3 Dentin block, the dentin block is dissolved in 2ml of phosphoric acid solution with a weight percentage of 85%, slowly shaken and soaked in a shaking table at a temperature of 4°C for three days to obtain a reaction solution, and then the resulting reaction solution is heated at 4°C and 1200rpm Centrifuge and separate, take the supernatant to obtain the dentin demineralization solution, and store it at 4°C for later use;

[0021] 2) Add 0.5 ml of 30% hydrogen peroxide to the dentin demineralization solution, stir and mix evenly, and perform foaming treatment;

[0022] 3) Add calcium hydroxide powder with a particle size of 2-10 μm to the dentin demineralization solution after foaming treatment, stir while adding, and detect the pH value of the reactant by potentiometric method, stop adding hydrogen until the pH i...

Embodiment 2

[0027] 1) Take the caries-free premolars extracted for orthodontic treatment, remove the roots and enamel, and cut them into 2*2*1.5mm by using a high-speed turbine 3 Dentin block, the dentin block is dissolved in 2ml of phosphoric acid solution with a weight percentage of 90%, slowly shaken and soaked in a shaking table at a temperature of 4°C for three days to obtain a reaction solution, and then the resulting reaction solution is heated at 4°C, 1200rpm Centrifuge and separate, take the supernatant to obtain the dentin demineralization solution, and store it at 4°C for later use;

[0028] 2) Add 0.4ml of 40% hydrogen peroxide by weight to the dentin demineralization solution, stir and mix evenly, and perform foaming treatment;

[0029] 3) Add calcium hydroxide powder with a particle size of 2-10 μm to the dentin demineralization solution after foaming treatment, stir while adding, and detect the pH value of the reactant by potentiometric method, stop adding hydrogen until th...

Embodiment 3

[0033] 1) Take the caries-free premolars extracted for orthodontic treatment, remove the roots and enamel, and cut them into 2*2*1.5mm by using a high-speed turbine 3 2 pieces of dentin blocks, the dentin blocks were dissolved in 4ml of phosphoric acid solution with a weight percentage of 70%, slowly shaken and soaked in a shaking table at a temperature of 4°C for three days to obtain a reaction solution, and then the resulting reaction solution was placed at 4°C, Centrifuge at 1200rpm, take the supernatant to obtain the dentin demineralization solution, and store it at 4°C for later use;

[0034] 2) Add 1ml of 20% hydrogen peroxide by weight to the dentin demineralization solution, stir and mix evenly, and perform foaming treatment;

[0035]3) Add calcium hydroxide powder with a particle size of 2-10 μm to the dentin demineralization solution after foaming treatment, stir while adding, and detect the pH value of the reactant by potentiometric method, stop adding hydrogen unti...

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Abstract

The invention discloses a preparation method of an odontal restoration material, which comprises the following steps: dentin blocks are taken to be dissolved into phosphoric acid solution with the weight percentage of 70-90%, supernatant liquor is taken after the centrifugal treatment, so the dentin demineralization solution is obtained; then hydrogen peroxide with the weight percentage of 20-40%is added into the dentin demineralization solution to carry out the foaming treatment; calcium hydroxide powder is added into the dentin demineralization solution after the foaming treatment, adding and mixing are carried out at the same time until the pH of the reactant is 7, so the pasty odontal restoration raw material is obtained; the odontal restoration raw material undergoes the microwave treatment, and the treatment time is controlled between 20 and 40min; and finally, the odontal restoration raw material is dried at the constant temperature of 37 DEG C, so the odontal restoration material is obtained. Practice shows that the method has low cost and is simple to operate, the reaction condition is moderate, and the produced odontal restoration material has good excellent performance.

Description

technical field [0001] The invention relates to the field of preparation of medical biological materials, in particular to a preparation method of a tooth restoration material. Background technique [0002] Caries is a common oral disease in humans, and its progression will eventually lead to the loss of dental hard tissues and seriously affect people's daily life. Clinically, the traditional treatment methods for dental caries are mechanical caries removal, cavity preparation and cavity filling with restorative materials. Dental hard tissues are mainly composed of inorganic hydroxyapatite crystals (Ca 10 (PO 4 ) 6 (OH) 2 ) and a small amount of organic matrix, hydroxyapatite crystals are arranged in an orderly manner under the control of organic matrix proteins (this process is called biomineralization), and dentin with unique internal structure and physical characteristics is obtained. When using the method of filling the cavity, restorative materials that are similar...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K6/02A61K6/033A61K6/838
Inventor 周彬刘燕
Owner TONGJI HOSPITAL ATTACHED TO TONGJI MEDICAL COLLEGE HUAZHONG SCI TECH