Fast drying ampholytic polymers for cleaning compositions
A technology of hard surface cleaners and terpolymers, applied in detergent compositions, organic detergent compositions, cationic surface active compounds, etc., which can solve the problems of slow drainage of water film and increased time required for surface drying
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[0170] The 1 L reactor was purged with nitrogen. An initial charge of 15.5 g DADMAC (65.9%) solution, 1.3 g N,N-dimethylacrylamide, 40 mg acrylic acid (99%) solution, 1.5 g NaEDTA (10%) solution and 250 g deionized water was added to the reactor. The pH of the reaction mixture was adjusted to about 4.0 + / - 0.2 with HCl (5%) solution. The reaction was stirred at 210 rpm and heated to 100°C. A monomer charge was prepared from 6.7 g DADMAC (65.9%) solution, 54 g N,N-dimethylacrylamide, 3.25 g acrylic acid (99%) solution, 70 mg thioglycolic acid and 110 g deionized water. The pH of the feed solution was adjusted to about 4.0 + / - 0.2 with NaOH (10%) solution. Initially 5 ml of the monomer feed was added to the reactant mixture. Initiator (ammonium persulfate, 0.2 g in 20 ml of water) was introduced at a rate of 0.22 ml / min while the remainder of the monomer feed was added over 60 min. After completion of the monomer feed, the container containing the monomer feed was rinsed wit...
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