Method for preparing isometric crystal high temperature alloy casting alloy/ceramic interface reaction test sample
A high-temperature alloy and interface reaction technology, which is applied in the field of high-temperature alloy precision casting, can solve problems such as low test efficiency, error, and inability to judge the reaction time, and achieve the effects of improving test efficiency, improving test efficiency, and saving test materials
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Embodiment 1
[0023] The equiaxed crystal hollow casting is made of nickel-based superalloy K4648 with high Cr content. The concrete steps that adopt technical scheme of the present invention are as follows:
[0024] (1) Preparation of shell type
[0025] A shell mold for directional solidification with two ceramic cores inside is prepared by traditional investment casting technology;
[0026] (2) Heating and insulation of shell type
[0027] Heat the shell in the heater of the directional solidification vacuum induction furnace to the temperature at which the alloy / ceramic interface reaction is expected to occur, set the temperature at 800°C, and keep it warm for 10 minutes;
[0028] (3) Remelting and pouring
[0029] Remelt the high-temperature alloy ingot, and when the holding time of the shell mold reaches 10 minutes, pour the alloy liquid into the cavity of the shell mold at a temperature not lower than the alloy liquidus line, and the pouring temperature is 1500°C;
[0030] (4) Di...
Embodiment 2
[0035] The equiaxed crystal hollow casting is made of nickel-based superalloy K4648 with high Cr content. The concrete steps that adopt technical scheme of the present invention are as follows:
[0036] (1) Preparation of shell mold: a shell mold for directional solidification with 6 ceramic cores inside is prepared by traditional investment casting process;
[0037] (2) Heating and heat preservation of the shell: heat the shell in the heater of the directional solidification vacuum induction furnace to the temperature at which the alloy / ceramic interface reaction is expected to occur, set the temperature at 1500°C, and keep it warm for 30 minutes:
[0038] (3) Remelting and pouring
[0039] Remelt the high-temperature alloy ingot, and when the holding time of the shell mold reaches 30 minutes, pour the alloy liquid into the cavity of the shell mold at a temperature not lower than the alloy liquidus line, and the pouring temperature is 1500°C;
[0040] (4) Directional solidi...
Embodiment 3
[0045] The material of the equiaxed crystal hollow casting is high-Cr content cast nickel-base superalloy K4648, and the specific steps of adopting the technical solution of the present invention are as follows:
[0046] (1) Preparation of shell type
[0047] A shell mold for directional solidification with 6 ceramic cores inside is prepared by traditional investment casting technology;
[0048] (2) Heating and heat preservation of the shell: heat the shell in the heater of the directional solidification vacuum induction furnace to the temperature at which the alloy / ceramic interface reaction is expected to occur, set the temperature at 1550 ° C, and keep it warm for 30 minutes;
[0049] (3) Remelting and pouring
[0050] Remelt the high-temperature alloy ingot, and when the holding time of the shell mold reaches 30 minutes, pour the alloy liquid into the cavity of the shell mold at a temperature not lower than the alloy liquidus line, and the pouring temperature is 1550°C; ...
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