Testing device for simulating equipment corrosion of continuous distillation industrial device

A technology for testing equipment and equipment corrosion, applied in measurement equipment, weather resistance/light resistance/corrosion resistance, instruments, etc., can solve the problems of insufficient understanding of the characteristics of vacuum distillation process, corrosion of oil refining equipment, and lack of light components.

Active Publication Date: 2012-05-09
CHINA PETROLEUM & CHEM CORP +1
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Heavy crude oil has high acid value, less light components, high density and viscosity, high colloidal asphaltene content, high salt content and heavy metal content, which seriously corrodes oil refining equipment, especially crude oil primary processing equipment, such as atmospheric and vacuum distillation units Directly subject to severe corrosion impact, but the industry has few ways to deal with it. The most important reason is the lack of understanding of the characteristics of the vacuum distillation process

Method used

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  • Testing device for simulating equipment corrosion of continuous distillation industrial device
  • Testing device for simulating equipment corrosion of continuous distillation industrial device

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Embodiment Construction

[0023] see figure 1 , the test device mainly includes continuous distillation system, pressure control system, corrosion sample system. The continuous distillation system includes a multi-necked flask 1, a main reactor 3, and a main condenser 7. The pressure control system includes a non-condensable gas receiving tank 10, a cold trap 11, and a vacuum pump 19. Sample hanging device for placing samples in phase and liquid phase. The multi-necked flask 1 is used to contain the medium used in the experiment, such as the crude oil after electric desalting or the bottom oil of the atmospheric distillation tower. There is an electric heater (not shown) conforming to the shape of the multi-necked flask 1 outside the multi-necked flask to heat the experimental medium in the flask. The main interface on the upper part of the multi-necked flask is connected with a cylindrical main reactor 3 made of glass. The upper end of the main reactor 3 is connected to a double-layer silver-plated...

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Abstract

The invention relates to a testing device for simulating the equipment corrosion of a continuous distillation industrial device. The testing device comprises a continuous distillation system, a pressure control system and a corrosion sample system, wherein the top interface of a multi-mouth flask is connected with the bottom of a main reactor; the top interface of the main reactor is connected with the bottom of a main condenser; the top of the main condenser is connected with a non-condensable gas receiving tank, a cold trap, a gas buffering tank and an exhaust system through connecting pipes respectively, and is connected to a vacuum pump through the cold trap; and the corrosion sample system comprises a sample hanging device for placing samples into a steam phase and a liquid phase. A skillful reflow design is adopted in the invention, so that a condensed low-boiling-point liquid does not flow through the high-temperature main reactor, so that re-vaporization before reflowing to the bottom of the multi-mouth flask is avoided. Under the action of a reflow bypass, condensed low-boiling-point components and high-boiling-point components left at the bottom of the multi-mouth flask are fully mixed forcedly, and the distillation process is started once again, so that accurate simulation of continuous distillation is realized.

Description

technical field [0001] The invention relates to an equipment corrosion test device for simulating a continuous distillation industrial device in a petroleum refining process. Background technique [0002] Atmospheric and vacuum distillation is the most important chemical separation process in the primary process of petroleum refining. With the deterioration of crude oil worldwide, it is mainly manifested in the increase of acid content and the increase of the proportion of heavy crude oil. Heavy crude oil has high acid value, less light components, high density and viscosity, high colloidal asphaltene content, high salt content and heavy metal content, which seriously corrodes oil refining equipment, especially crude oil primary processing equipment, such as atmospheric and vacuum distillation units It is directly affected by severe corrosion, but the industry has few ways to deal with it. The most important reason is the lack of understanding of the characteristics of the ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N17/00
Inventor 屈定荣刘小辉蒋秀
Owner CHINA PETROLEUM & CHEM CORP
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