Novel preparation method of starch-acrylamide grafted copolymer
A technology of graft copolymer and acrylamide, which is applied in the field of new preparation of starch-acrylamide graft copolymer, can solve the problems of molecular weight reduction, slow reaction speed, fast product reaction speed, etc., so as to improve the conversion rate of polymerization reaction and The effects of polymer intrinsic viscosity, reduced synthesis cost, and simple synthesis steps
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[0036] The novel preparation method of a kind of starch-acrylamide graft copolymer that the present invention relates to, its concrete steps are as follows:
[0037] (a) take starch and distilled water, place in reaction vessel, place reaction vessel in water bath;
[0038] (b) Install the stirring device and start stirring;
[0039] (c) feed nitrogen to remove the oxygen of the starch liquid in the reaction vessel;
[0040] (d) heating up and keeping it for a period of time to make the soluble starch gelatinize completely;
[0041] (e) system is cooled to reaction temperature;
[0042] (f) Continue to feed nitrogen into the gelatinized and cooled starch liquid, add an initiator, and the concentration of the initiator is 1.4mmol / L-1.6mmol / L, stir, and then add a certain amount of acrylamide monomer;
[0043] (g) Stirring is continued, and the starch and acrylamide are polymerized within a specified time to obtain a starch-acrylamide graft copolymer product.
[0044] In the s...
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