Method for preparing yttrium-doped nano aluminum nitride powder
A nano-aluminum nitride and yttrium-doped technology, which is applied in the field of material science, can solve problems such as the difficulty in achieving uniform mixing of additives and matrix materials, reducing the thermal conductivity of aluminum nitride ceramics, and increasing the content of sintering additives. Adverse effects, high density, effect of promoting dense sintering
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[0024] Example 1:
[0025] Weigh 1.0 mol aluminum nitrate dissolved in 2.0 L of deionized water to form a 0.5 mol / L aluminum source solution, and weigh 0.0076 mol of yttrium nitrate dissolved in 0.0152 L of deionized water to form a 0.5 mol / L yttrium source solution. The solution and the yttrium source solution are mixed to form an aluminum-yttrium mixed solution. Weigh 1.0 mol citric acid and dissolve it in 5.0 mol ethylene glycol, mix and stir evenly, and add it to the aluminum-yttrium mixed solution. Weigh 0.83 mol of glucose and dissolve it in 1.66 L of deionized water to form a 0.5 mol / L carbon source solution, mix it evenly and add it to the above-mentioned aluminum-yttrium mixed solution. Stir the above mixed solution evenly, then heat to 130 ℃ for 2 h, continue to heat to 200 ℃ for 2 h, after cooling, a fluffy brown-black powder is obtained. The above fluffy brown-black powder is calcined in a nitrogen atmosphere at 1000 ℃ for 1 h to obtain a uniformly mixed carbotherma...
Example Embodiment
[0026] Example 2:
[0027] Weigh 1.0 mol of aluminum acetate dissolved in 1.0 L of absolute ethanol to form a 1.0 mol / L aluminum source solution, and weigh 0.023 mol of yttrium nitrate dissolved in 0.023 L of absolute ethanol to form a 1.0 mol / L yttrium source solution. The aluminum source solution and the yttrium source solution are mixed to form an aluminum-yttrium mixed solution. Weigh 2.0 mol of citric acid and dissolve it in 8.0 mol of ethylene glycol, mix and stir evenly, and add to the above-mentioned aluminum-yttrium mixed solution. Weigh 0.8 mol of sucrose and dissolve it in 0.8 L of absolute ethanol to form a 1.0 mol / L carbon source solution, mix it evenly and add it to the above-mentioned aluminum-yttrium mixed solution. Stir the above mixed solution uniformly, then heat to 125 ℃ for 3 h, continue to heat to 180 ℃ for 4 h, after cooling, a fluffy brown-black powder is obtained. The above fluffy brown-black powder was calcined in a nitrogen atmosphere at 900 ℃ for 1 h...
Example Embodiment
[0028] Example 3:
[0029] Weigh 1.0 mol aluminum isopropoxide and dissolve it in 0.5 L acetone to form a 2.0 mol / L aluminum source solution, and weigh 0.03 mol yttrium acetate to dissolve in 0.03 L acetone to form a 1.0 mol / L yttrium source solution. The solution and the yttrium source solution are mixed to form an aluminum-yttrium mixed solution. Weigh 1.5 mol of citric acid and dissolve it in 8.0 mol of ethylene glycol, mix and stir evenly, and add to the above-mentioned aluminum-yttrium mixed solution. Weigh 0.3 mol glucose and 0.3 mol sucrose to dissolve in 1.2 L deionized water to form a 0.5 mol / L carbon source solution, mix them evenly and add them to the aluminum-yttrium mixed solution. Stir the above mixed solution evenly, then heat to 125 ℃ for 2 h, continue to heat to 220 ℃ for 2 h, after cooling, a fluffy brown-black powder is obtained. The above fluffy brown-black powder was calcined in a nitrogen atmosphere at 800 ℃ for 1 h to obtain a uniformly mixed carbothermic...
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