A kind of iron-based nanocrystalline soft magnetic alloy and preparation method thereof
A technology of iron-based nanocrystalline and soft magnetic alloys, applied in the field of alloys, can solve the problems of limited applications, large volume, low (up to 1.4T, usually around 1.2T), etc., to achieve high saturation magnetic induction and low loss Effect
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Embodiment 1
[0017] Ferro-silicon, ferro-boron, ferro-phosphorus, iron, copper, aluminum and other raw materials are configured in a certain proportion as Fe 82 Cu 0.5 al 1 Si 4.5 B 8 P 4 The masterbatch is 5 kg in total; the prepared masterbatch is added to the crucible of the vacuum intermediate frequency induction furnace for melting, and the intermediate frequency induction melting is carried out three times to obtain an alloy ingot with uniform composition; the alloy ingot is mechanically crushed and put into the quartz tube of the quenching belt making equipment In the process, induction heating and melting were adopted, and a single-roller quenching strip process was used to make strips at a speed of 35m / s in the air to obtain an amorphous thin strip with a strip width of 10mm and a thickness of 30 microns; the amorphous alloy strip Put into tube type vacuum heat treatment furnace, vacuum degree is at 10 -3 Around Pa, raise the temperature to 360°C at a heating rate of 15°C / min...
Embodiment 2
[0019] Ferro-silicon, ferro-boron, ferro-phosphorus, iron, copper, aluminum and other raw materials are configured in a certain proportion as Fe 80 Cu 0.5 al 1.5 Si 5 B 9 P 4 The masterbatch is 5 kg in total; the prepared masterbatch is added to the crucible of the vacuum intermediate frequency induction furnace for melting, and the intermediate frequency induction melting is carried out three times to obtain an alloy ingot with uniform composition; the alloy ingot is mechanically crushed and put into the quartz tube of the quenching belt making equipment In the process, induction heating and melting were adopted, and a single-roller quenching strip process was used to make strips at a speed of 35m / s in the air to obtain an amorphous thin strip with a strip width of 10mm and a thickness of 30 microns; the amorphous alloy strip Put into tube type vacuum heat treatment furnace, vacuum degree is at 10 -3 Around Pa, raise the temperature to 360°C at a heating rate of 15°C / min...
Embodiment 3
[0021] Ferro-silicon, ferro-boron, ferro-phosphorus, iron, copper, aluminum and other raw materials are configured in a certain proportion as Fe 78.5 Cu 0.5 al 2 Si 5.5 B 9.5 P 4 The masterbatch is 5 kg in total; the prepared masterbatch is added to the crucible of the vacuum intermediate frequency induction furnace for melting, and the intermediate frequency induction melting is carried out three times to obtain an alloy ingot with uniform composition; the alloy ingot is mechanically crushed and put into the quartz tube of the quenching belt making equipment In the process, induction heating and melting were adopted, and a single-roller quenching strip process was used to make strips at a speed of 35m / s in the air to obtain an amorphous thin strip with a strip width of 10mm and a thickness of 30 microns; the amorphous alloy strip Put into tube type vacuum heat treatment furnace, vacuum degree is at 10 -3 Around Pa, raise the temperature to 360°C at a heating rate of 15°C...
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