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Manufacturing method of led electrode using ito/zno based composite film as p electrode

A fabrication method and p-electrode technology, applied in circuits, electrical components, semiconductor devices, etc., can solve the problems of inability to form an ITO/ZnO-based composite film electrode area, unsatisfactory, fast corrosion rate, etc., to reduce material costs, flexible High performance and simple preparation process

Inactive Publication Date: 2015-08-26
ZHEJIANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the process of etching the ITO / ZnO-based composite film by photolithography, the ZnO-based conductive film not protected by the photoresist is corroded first, exposing the ITO conductive film, and as the etching time progresses, the exposed ITO conductive film However, due to the fast corrosion rate of the ZnO-based conductive film, while corroding the exposed ITO conductive film, part of the ZnO-based conductive film in the photoresist protection part will also be corroded, and even ZnO-based conductive film will appear. If the film is completely corroded but the ITO conductive film has not been corroded, the electrode area covered by the ITO / ZnO-based composite film cannot be formed, which cannot meet the needs of actual production

Method used

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  • Manufacturing method of led electrode using ito/zno based composite film as p electrode
  • Manufacturing method of led electrode using ito/zno based composite film as p electrode
  • Manufacturing method of led electrode using ito/zno based composite film as p electrode

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Embodiment 1

[0039] See attached Figure 1~12 , the preparation method of the present invention comprises the following steps:

[0040] 1) if figure 1 Shown: conventional acid cleaning, organic cleaning, and water cleaning are performed on the substrate 1;

[0041] 2) if figure 2 As shown: put the cleaned substrate 1 into the ITO evaporation table, and evaporate a 100nm thick ITO conductive film 2 at a temperature of 350°C and oxygen;

[0042] 3) if image 3 As shown: uniformly coat photoresist 8 on the substrate 1 on which the ITO conductive film 2 is deposited, perform photolithography, and etch out the window 9 of the ITO conductive film;

[0043] 4) if Figure 4 As shown: the ITO conductive film 2 is corroded by concentrated hydrochloric acid with a mass concentration of 37%, the ITO conductive film 2 exposed by the window 9 is corroded by the etching solution, and the n-electrode region 7 is exposed, and the ITO conductive film 2 outside the window 9 is covered by the photoresis...

Embodiment 2

[0052] See attached Figure 1~12 , the preparation method of the present invention comprises the following steps:

[0053] 1) if figure 1 Shown: conventional organic cleaning and water cleaning are performed on the substrate 1;

[0054] 2) if figure 2 As shown: put the cleaned substrate 1 into the ITO evaporation table, and evaporate a 20nm thick ITO conductive film 2 at a temperature of 250°C and oxygen;

[0055] 3) if image 3 As shown: uniformly coat photoresist 8 on the substrate 1 on which the ITO conductive film 2 is deposited, perform photolithography, and etch out the window 9 of the ITO conductive film;

[0056] 4) if Figure 4 As shown: the ITO conductive film 2 is corroded by concentrated hydrochloric acid with a mass concentration of 37%, the ITO conductive film 2 exposed by the window 9 is corroded by the etching solution, and the n-electrode region 7 is exposed, and the ITO conductive film 2 outside the window 9 is covered by the photoresist 8 protection, ...

Embodiment 3

[0065] See attached Figure 1~12 , which plots the fabrication process of one embodiment of the invention.

[0066] 1) if figure 1 Shown: conventional acid cleaning and organic cleaning are performed on the substrate 1;

[0067] 2) if figure 2 As shown: put the cleaned substrate 1 into the ITO evaporation table, and evaporate a 50nm thick ITO conductive film 2 at a temperature of 300°C and oxygen;

[0068] 3) if image 3 As shown: uniformly coat photoresist 8 on the substrate 1 on which the ITO conductive film 2 is deposited, perform photolithography, and etch out the window 9 of the ITO conductive film;

[0069] 4) if Figure 4 As shown: sulfuric acid with a mass concentration of 15% is used to etch the ITO conductive film 2, the ITO conductive film 2 exposed by the window 9 is corroded by the etching solution, and the n-electrode region 7 is exposed, and the ITO conductive film 2 outside the window 9 is covered by the photoresist 8 Protected from being corroded by the...

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Abstract

The invention discloses a method for preparing an LED (light-emitting diode) electrode taking an ITO / ZnO based composite film as a p electrode, and the method comprises the following steps: 1) cleaning a substrate; 2) depositing an ITO conductive film on the substrate; 3) photoetching the ITO conductive film so as to form an n electrode area and a p electrode area which is covered by the ITO conductive film, wherein the ITO conductive film covered area is slightly larger than the p electrode area; 4) depositing a ZnO based conductive film on the n electrode area and the p electrode area; 5) photoetching the ZnO based conductive film, and removing the ZnO film on the n electrode area, and forming an ITO / ZnO based composite film on the p electrode area; 6) etching a step on the n electrode area; 7) sequentially depositing an electrode metal and a passivation layer on the step of the n electrode area and the ITO / ZnO based composite film, wherein the passivation layer covers the electrode metal; and 8) removing the passivation layer on the electrode metal through etching so as to obtain an LED electrode taking an ITO / ZnO based composite film as the p electrode. The method disclosed by the invention is good in processing effect, high in product reliability, simple in preparation process, and easy to popularize and use.

Description

technical field [0001] The invention relates to a method for manufacturing an electrode of a light-emitting diode, in particular to a method for manufacturing an LED electrode using an ITO / ZnO-based composite film as a p-electrode. Background technique [0002] Due to the dual advantages of energy saving and environmental protection, light-emitting diodes (LEDs) are considered to be the most promising new generation of energy-saving lighting sources in the 21st century, and have been widely used. However, the preparation methods of LEDs still need to be continuously improved, mainly to reduce cost and improve luminous efficiency. The p-electrode material commonly used in LEDs is Ni / Au, but Ni / Au is opaque, which affects the luminous efficiency of LEDs. If transparent electrodes are used, the luminous efficiency will be significantly improved. [0003] At present, indium tin oxide (ITO) is mainly used as the transparent electrode material of LED. However, since In is a rare ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01L33/00
Inventor 吕建国陈丹叶志镇
Owner ZHEJIANG UNIV