Liquid-phase dispersion white carbon black latex mixture contained mine tire tread rubber compound and preparation method and application thereof
A liquid phase dispersion and white carbon black technology, which is applied in special tires, tire parts, transportation and packaging, etc., can solve the problems of heat generation performance decline, tread hysteresis loss increase, durability deterioration and other problems
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Embodiment 1
[0069] Centrifugal concentration of natural rubber latex and silica slurry
[0070] A. Preparation of slurry
[0071] A component
[0072] formula composition(%) Silica slurry (25% content) 85.47 water 13.33 Si69 0.66 stabilizer 0.410 Anti-settling agent 0.020 Dispersant 0.103
[0073] B component
[0074] formula composition(%) Concentrated Natural Rubber Latex 56.31 stabilizer 0.54 water 43.15
[0075] Each was stirred at 1500~2500rpm for 2~5 minutes.
[0076] B. Mix and stir, slowly add component A to component B while stirring at a high speed, the mass ratio of component A to component B is 0.8:1, the stirring speed is 2000~6000rpm, and stir for 10 minutes.
[0077] C. Slowly add 0.3kg of glacial acetic acid to the mixture and solidify instantly.
[0078] D. Press filtration, press on the press, squeeze out part of the liquid, and recycle.
[0079] E. Rolling, rollin...
Embodiment 2
[0085] Using fresh glue and silica paste collected directly from rubber trees
[0086] A. Preparation of slurry
[0087] A component
[0088] formula composition(%) Silica slurry (25% content) 85.47 water 13.33 Si69 0.66 stabilizer 0.410 Anti-settling agent 0.020 Dispersant 0.103
[0089] B component
[0090] formula composition(%) fresh glue 99.056 stabilizer 0.944 water
[0091] Each was stirred at 1500~2500rpm for 2~5 minutes.
[0092] B. Mix and stir, slowly add component A to component B while stirring at a high speed, the mass ratio of component A to component B is 1:1, the stirring speed is 2000~6000rpm, and stir for 10 minutes.
[0093] C. Slowly add 0.3kg of glacial acetic acid to the mixture and solidify instantly.
[0094] D. Press filtration, press on the press, squeeze out part of the liquid, and recycle.
[0095] E. Rolling, rolling 3 to 5 times on a rubber...
Embodiment 3~5
[0101] Containing the mine tire tread rubber material of the liquid-phase dispersed silica latex mixture, the rubber material includes the components in the following table in parts by weight, wherein the comparative example is formed by mixing natural rubber and carbon black, and the examples 3~ 5 is obtained by mixing the liquid-phase dispersed silica latex mixture (represented by LNSC in the table) prepared in Example 1 or Example 2 with or without adding natural rubber and carbon black.
[0102]
[0103]
[0104] The mining tire tread rubber compound containing the liquid-phase dispersed silica latex mixture of the above-mentioned embodiments 3 ~ 5 is prepared by mixing according to the following method:
[0105] (1) Plasticizing section
[0106] Add liquid-phase dispersed silica latex mixture, stearic acid, zinc oxide, microcrystalline wax, anti-aging agent RD and anti-aging agent 4020, the rotor speed is 45rpm, press the lump and keep it at 140°C, lift the lump and o...
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