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Preparation method and device of high-softening-point asphalt, high-softening-point asphalt, and binding agent prepared from high-softening-point asphalt

A technology of high softening point asphalt and preparation device, which is applied in the direction of melting and processing tar asphalt/petroleum asphalt/natural asphalt, chemically processing tar asphalt/petroleum asphalt/natural asphalt, and asphalt material binder, etc. Uniform and high softening point special asphalt quality is not stable enough, the average softening point of asphalt is not high, etc., to achieve the effect of stable quality index

Active Publication Date: 2013-01-16
山东杰富意振兴化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, when heating in the existing reactor, the modified asphalt itself is relatively viscous and has poor thermal conductivity. Therefore, when the temperature in the reactor is raised, the temperature of the modified asphalt itself is difficult to control properly, resulting in poor heating. In general, the quality of the produced high softening point special asphalt is not stable enough, that is, the softening point of the product cannot be controlled within a narrow range
Also because of this reason, the average softening point of asphalt is generally not high at present. When the required softening point is higher, the softening point of the asphalt will not be controlled within a narrow range due to uneven heating.

Method used

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  • Preparation method and device of high-softening-point asphalt, high-softening-point asphalt, and binding agent prepared from high-softening-point asphalt

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] The preparation method of high softening point asphalt, the step comprises:

[0036] S1. Import the modified pitch into the monomer container 1, and pass an inert gas into the monomer container 1. The inert gas is nitrogen, and the heating temperature of the four-stage electric heater 3 is sequentially adjusted from top to bottom to 253°C, 257°C, 259°C and 260°C, and turn on the heating to keep the pressure in the monomer container 1 at 0.03MPa;

[0037] S2. After the modified asphalt is heated to 250° C., the temperature is maintained for 13 hours to obtain the high softening point asphalt.

[0038] Finally, the softening point of the high softening point pitch prepared in this example is 250°C, the fixed carbon content is 81%wt, and the ash content is 0.5%wt.

[0039] Utilize this high softening point pitch as raw material to prepare binding agent, after measuring, the softening point of described binding agent is 250 ℃, and fixed carbon content is 80%wt, and ash con...

Embodiment 2

[0041] The preparation method of high softening point asphalt, the step comprises:

[0042] S1. Import the modified asphalt into the monomer container 1, and pass an inert gas into the monomer container 1. The inert gas is nitrogen, and the heating temperature of the four-stage electric heater 3 is adjusted to 354°C from top to bottom. , 355°C, 356°C and 358°C, and turn on the heating to keep the pressure in the monomer container 1 at 0.04MPa;

[0043]S2. After the modified asphalt is heated to 350° C., the temperature is maintained to continue the reaction for 16 hours to obtain the high softening point asphalt.

[0044] Finally, the softening point of the high softening point pitch prepared in this example is 350°C, the fixed carbon content is 87%wt, and the ash content is 0.45%wt.

[0045] Using the high softening point pitch as raw material to prepare a binder, the softening point of the binder is determined to be 350°C, the fixed carbon content is 86%wt, and the ash cont...

Embodiment 3

[0047] The preparation method of high softening point asphalt, the step comprises:

[0048] S1. Import the modified asphalt into the monomer container 1, and pass an inert gas into the monomer container 1. The inert gas is nitrogen, and the heating temperature of the four-stage electric heater 3 is adjusted to 375°C from top to bottom. , 376°C, 378°C and 382°C, and turn on the heating to keep the pressure in the monomer container 1 at 0.05MPa;

[0049] S2. After the modified asphalt is heated to 370° C., the temperature is maintained for 18 hours to obtain the high softening point asphalt.

[0050] Finally, the softening point of the high softening point pitch prepared in this example is 370°C, the fixed carbon content is 89%wt, and the ash content is 0.42%wt.

[0051] A binder was prepared using the high softening point pitch as a raw material. After measurement, the softening point of the binder was 250°C, the fixed carbon content was 88%wt, and the ash content was 0.42%wt....

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Abstract

The invention provides a preparation method of high-softening-point asphalt, which comprises the following steps: introducing modified asphalt into a single container, and introducing inert gas into the single container, wherein the single container is sequentially provided with at least three independent heating zones from top to bottom, an independent heater is arranged in each heating zone, the heating temperatures gradually increase, and the reaction pressure is 0.03-0.05 MPa; and after heating the modified asphalt to the target temperature, keeping the temperature for 6-18 hours, thereby obtaining the high-softening-point asphalt. The invention also provides a preparation device, a prepared high-softening-point asphalt and a binding agent prepared from the high-softening-point asphalt. The invention can control the softening point of the modified asphalt within a narrow range, so that the modified asphalt has more stable quality, and the high-softening-point asphalt and binding agent with high softening point and high fixed carbon content can be prepared.

Description

technical field [0001] The invention relates to the preparation of high softening point asphalt, in particular to a process for preparing high softening point asphalt by heating a monomer container and the equipment used. Background technique [0002] At present, modified asphalt is a product obtained after deep processing of coal tar, which is a product obtained by atmospheric distillation and vacuum distillation of coal tar. [0003] Now, as the requirements for the environment and energy are getting higher and higher, small-scale steelmaking blast furnaces are gradually being eliminated, and the softening point of refractory binders currently used in the market to repair steelmaking blast furnaces is generally 150°C ~160°C, and the carbon content is very low, so it is unstable at high temperatures. With the increasing scale of steelmaking blast furnaces and higher working temperatures, the current refractory binders have far reached Less than required. Asphalt is one of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10C3/02C10C3/10C10C3/12C09J195/00
Inventor 杨建杰郑伟
Owner 山东杰富意振兴化工有限公司
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