Method and apparatus for separating two adhered plates, and pressure-sensitive adhesive sheet
A technology of pressure-sensitive adhesive sheets, silicone pressure-sensitive adhesive sheets, applied in the direction of bonding methods, pressure-sensitive films/sheets, adhesives, etc.
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Embodiment 1
[0204]
[0205] Prepare slurry mixture 1
[0206] The monomer solution was put into a reaction vessel with a condenser, a thermometer and a stirrer, and hydrogenated xylylene diisocyanate (manufactured by Takeda Pharmaceutical Company Limited, Takenate 600, hereinafter abbreviated as "HXDI", 12.4 parts by weight) so that the mixture was reacted at 65° C. for 4 hours, the monomer solution containing 2-ethylhexyl acrylate (produced by TOAGOSEI CO. , LTD.), hereinafter abbreviated as "2EHA", 173.2 parts by weight), ADEKA (registered trademark) pluronic L-62 (molecular weight 2500, manufactured by Adico Corporation, polyether polyol) as polyoxyalkylene polypropylene glycol , 100 parts by weight) and dibutyltin dilaurate (manufactured by KISHIDA CHEMICAL Co., Ltd., hereinafter abbreviated as "DBTL", 0.014 parts by weight) as a polyurethane catalyst. The content ratio of the polyisocyanate component to the polyol component used was NCO / OH (equivalent ratio)=1.6. Thereafter, 2-hy...
Embodiment 2
[0210]
[0211] Except for using IBXA instead of 2EHA as the unsaturated ethylene monomer, in the same manner as in Example 1 to prepare the slurry mixture, a hydrophilic polyurethane polymer / unsaturated ethylene polymer having acryloyl groups on both ends was obtained. A slurry mixture of monomers. The obtained hydrophilic polyurethane polymer had a weight average molecular weight of 15,000. 2EHA (38.6 parts by weight), IBXA (55.1 parts by weight) and AA (10.7 parts by weight) were added to 100 parts by weight of the obtained hydrophilic polyurethane polymer / unsaturated ethylene monomer slurry mixture to provide hydrophilic polyurethane Polymer / Ethylenically Unsaturated Monomer Slurry Mixture 2.
[0212] Except using the hydrophilic urethane polymer / unsaturated ethylene monomer slurry mixture 2 obtained as above instead of the hydrophilic urethane polymer / unsaturated ethylene monomer slurry mixture 1 and using NK ester A-HD-N (16 parts by weight) and UA (47.6 parts by wei...
Embodiment 3~5、 comparative example 1~2
[0230] The above slip resistance evaluation test was carried out using the pressure-sensitive adhesive sheets for fixing shown in Table 2 below instead of the porous pressure-sensitive adhesive sheets.
[0231] Table 2
[0232]
Pressure sensitive adhesive sheet for fixing
Anti-slip evaluation results
Example 1
Porous pressure sensitive adhesive sheet A
⊙
Example 2
Porous pressure sensitive adhesive sheet B
○
Example 3
N-300
⊙
Example 4
No.3630H
○
Example 5
TRN-6250L
○
Comparative example 1
No.5000NS
×
Comparative example 2
dashboard storage slice
×
[0233] In Table 2, "N-300" is a silicone pressure-sensitive adhesive sheet (trade name "N-300", manufactured by NITTO DENKO CORPORATION), and "No. 3630H" is a silicone pressure-sensitive adhesive sheet Pressure-sensitive adhesive sheet (trade name "No.3630H", manufactured by Nitto Denko C...
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