Environment-friendly building material
A material composition and weight meter technology, applied in the field of building materials, can solve problems such as flammability, poor ecological environmental protection, poor stability, etc.
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Embodiment 1
[0028] Embodiment 1: the preparation of formula I compound
[0029] (1) Synthesis of (E)-4-(2-hydroxyphenyl)-3-buten-2-one
[0030]Add 2-hydroxybenzaldehyde (20.0mmol), 24mL acetone, and 10mL water successively in a 100mL three-necked flask, stir at room temperature until the solids are completely dissolved, and add a solution of sodium hydroxide (24mmol)+20mL water drop by drop, and the reaction solution consists of light The yellow clear liquid turns into a wine-red clear liquid, the reaction is complete, the acetone is removed by rotary evaporation, 70mL hot water is added to the residual liquid until the red solid is completely dissolved, and carbon dioxide is introduced for about 30 minutes until the reaction liquid no longer changes color, and a light yellow solid appears , filtered, washed with water, dried, and recrystallized with acetone / water to obtain a light yellow solid with a yield of 78.3% and a melting point of 137-139°C.
[0031] (2) Synthesis of (1E, 4E)-1-(...
Embodiment 2
[0040] Take 20 parts of rubber particles, 1 part of dicumyl peroxide, 3 parts of silica powder, 10 parts of aluminate refractory cement, 5 parts of polyacrylonitrile-based carbon fiber, 5 parts of carbon fiber, 5 parts of bentonite, 2 parts of magnesium oxide, as shown in formula I 2 parts compound, 3 parts perlite, 3 parts polyurethane foam, 100 parts water. Under the condition of rotating speed 800-1000 rpm, add water, aluminate refractory cement and silica powder in turn, and stir for 5 minutes; then add other components, adjust the rotating speed and stir for 10 minutes under the condition of 1000-1500 rpm, Then under the condition of 2000-2500 rev / min, stir for 10 minutes.
Embodiment 3
[0042] 25 parts of rubber particles, 2 parts of dicumyl peroxide, 5 parts of silica powder, 13 parts of aluminate refractory cement, 10 parts of polyacrylonitrile-based carbon fiber, 9 parts of carbon fiber, 8 parts of bentonite, 3 parts of magnesium oxide, formula I 4 parts of the indicated compound, 6 parts of perlite, 5 parts of polyurethane foam, and 100 parts of water. Under the condition of rotating speed 800-1000 rpm, add water, aluminate refractory cement and silica powder in turn, and stir for 5 minutes; then add other components, adjust the rotating speed and stir for 10 minutes under the condition of 1000-1500 rpm, Then under the condition of 2000-2500 rev / min, stir for 10 minutes.
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