Polyurethane grouting material and preparation method thereof
A grouting material, polyurethane technology, applied in the directions of reagents, educts, products, etc., can solve the problems of residual free TDI, environmental hazards, and high viscosity
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Embodiment 1
[0024]
[0025] The preparation method of one-component polyurethane grouting material is as follows:
[0026] In the interlayer reaction kettle, add polyether polyol and dioctyl phthalate according to the formula, dehydrate for 2 to 3 hours at a temperature of 110-120°C and a vacuum of -0.1MPa, and cool down to 60 ℃, add small molecule chain extender, stir evenly, add MDI, slowly raise the temperature to 85°C, react for two hours, cool down to below 30°C, add additives, stir evenly, then discharge, fill with nitrogen and seal the package. When using, open the package and use directly.
Embodiment 2
[0028]
[0029] The preparation method of one-component polyurethane grouting material is as follows:
[0030] In the interlayer reaction kettle, add polyether polyol and dioctyl phthalate according to the formula, dehydrate for 2 to 3 hours at a temperature of 110-120°C and a vacuum of -0.1MPa, and cool down to 60 ℃, add MDI-50, slowly raise the temperature to 85 ℃, react for two hours, cool down to below 30 ℃, add additives, stir evenly, discharge, fill with nitrogen and seal the package. When using, open the package and use directly.
Embodiment 3
[0032]
[0033] The preparation method of one-component polyurethane grouting material is as follows:
[0034] In the interlayer reaction kettle, add polyether polyol and dioctyl phthalate according to the formula, dehydrate for 2 to 3 hours at a temperature of 110-120°C and a vacuum of -0.1MPa, and cool down to 60 ℃, add PAPI, slowly raise the temperature to 75°C, react for two hours, cool down to below 30°C, add additives, stir evenly, discharge, fill with nitrogen and seal the package. When using, open the package and use directly.
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