Use of dispersions of iron particles as fuel additive
A technology of fuel additives and dispersions, which is applied in the direction of fuel additives, liquid carbon-containing fuels, fuels, etc., and can solve the problems of reduced oxidation resistance of fuels
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Embodiment 1
[0172] Example 1: Preparation of iron particles in crystalline form (according to the invention)
[0173] Preparation of solutions of iron precursors
[0174] Prepare 1 liter of solution in the following manner: 576 g Fe(NO 3 ) 3 with 99.4g FeCl 2 .4H 2 O mix. The mixture was completed with distilled water to obtain 1 L of solution. The final concentration of the iron precursor solution was 1.5 mol / L Fe.
[0175] Prepare Soda Solution
[0176] A 6 mol / L NaOH solution was prepared as follows: 240 g of soda flakes were diluted with distilled water to obtain 1 liter of solution.
[0177] In a 1-liter reactor equipped with a stirring system, a solution consisting of 400 ml of 3 mol / L sodium nitrate solution was introduced to the bottom of the tank. Add a few drops of 6 mol / L soda to adjust the pH of the solution to 13. A precipitate was formed by simultaneously adding the previously prepared iron precursor solution and the soda solution. The flow rates at which thes...
Embodiment 4
[0193] Example 4: Characterization of Iron Particle Dispersions
Embodiment 41
[0194] Example 4.1: X-ray Diffraction (XRD)
[0195] XRD analysis was performed according to the instructions given in the description.
[0196] It can be seen that the peaks of the diffraction patterns of the dispersion of Example 1 and the dispersion of Comparative Example 2 actually correspond to the XRD characteristics of the diffraction peaks of the crystalline magnetite phase and / or maghemite phase (Worksheet ICDD01-088- 0315).
[0197] The diffractogram of the dispersion of Comparative Example 3 does not have any distinct peaks, allowing conclusions to be drawn about the amorphous morphology of the iron phase.
[0198] Calculation of the crystallite size according to the method shown above yields a compatible crystallite size of 4 nm for Example 1 and an incompatible crystallite size of 9 nm for Comparative Example 2.
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