Anti-Fog Polyurethane Coating Composition
A composition and polyurethane technology, applied in polyurea/polyurethane coatings, coatings, thin material treatment, etc., can solve problems such as poor anti-fog coatings
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Embodiment 1
[0146] Embodiment 1-preparation of aqueous polyurethane dispersion with amphoteric surfactant
[0147] 21.1 grams of IPDI, 28.2 grams of PC2000, 2.1 grams of trimethylolpropane, 3.2 grams of dimethylolpropionic acid, 8.1 grams of Tegomer D3403 and 35 grams of methyl ethyl ketone were mixed together. The mixture was heated to 70°C and 0.01 g of tin catalyst was added. The mixture was then allowed to react for 3 hours under nitrogen atmosphere. After the reaction was finished, the obtained polyurethane prepolymer mixture was cooled to 40°C. 40.3 grams of the polyurethane prepolymer mixture was then dispersed into 51.2 grams of water and 7.0 grams of an aqueous betaine surfactant solution using a high shear disperser. 0.25 grams of hydrazine monohydrate and 0.58 grams of 1,6-hexanediamine were also added during dispersion with the high shear disperser to produce an aqueous polyurethane dispersion with a solids content of approximately 27% by weight of the dispersion. The res...
Embodiment 2
[0149] Embodiment 2-preparation of aqueous polyurethane dispersion with amphoteric surfactant
[0150] 24.7 grams of IPDI, 14.7 grams of PC2000, 3.2 grams of trimethylolpropane, 3.0 grams of dimethylolpropionic acid, 15.3 grams of PEO-side chain diol, 1.9 grams of PTF1000 and 35 grams of acetonitrile were mixed together. The mixture was heated to 70°C and 0.01 g of tin catalyst was added. The mixture was then allowed to react for 3 hours under nitrogen atmosphere. After the reaction was finished, the obtained polyurethane prepolymer mixture was cooled to 40°C. 40.9 grams of the polyurethane prepolymer mixture was then dispersed into 51.2 grams of water and 7.4 grams of the aqueous amine oxide surfactant solution using a high shear disperser. 0.55 grams of hydrazine monohydrate was also added during dispersion with the high shear disperser to produce an aqueous polyurethane dispersion with a solids content of approximately 28% by weight of the dispersion. The resulting pol...
Embodiment 3
[0152] Example 3 - Preparation of aqueous polyurethane dispersions with amphoteric surfactants
[0153] 22.0 grams of IPDI, 20.2 grams of PC2000, 2.1 grams of trimethylolpropane, 3.2 grams of dimethylolpropionic acid, 9.1 grams of PEO-side chain diol, 5.9 grams of PEG1000 and 35 grams of methyl ethyl ketone were mixed together. The mixture was heated to 70°C and 0.01 g of tin catalyst was added. The mixture was then allowed to react for 3 hours under nitrogen atmosphere. After the reaction was finished, the obtained polyurethane prepolymer mixture was cooled to 40°C. 37.2 grams of the polyurethane prepolymer mixture were then dispersed into 53.3 grams of water and 7.3 grams of the aqueous amine oxide surfactant solution using a high shear disperser. 0.25 grams of hydrazine monohydrate and 0.59 grams of 1,6-hexanediamine were also added during dispersion with the high shear disperser to produce an aqueous polyurethane dispersion with a solids content of approximately 27% by...
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