Printing ink for wash label and preparation method thereof
A technology of ink and glycerin, applied in the printing field, can solve problems such as poor fastness to rubbing, easy bleeding, and poor environmental protection of inks
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[0021] The embodiment of the present invention also discloses a preparation method of ink for washing labels, comprising the following steps:
[0022] S1. C.I. Direct Black 168, 2.5% to 3% C.I. Direct Black 19, 0.5% glycerin, 5% 1,3-dimethyl-3-imidazolinone, Add ionized water to 100% mix;
[0023] S2, heating and stirring the above mixture, then cooling, adding ethanol with a mass ratio of 3%, and continuing to stir;
[0024] S3. Using a membrane with a pore size of 0.4 μm, vacuum filtration to obtain the ink.
[0025] Washing mark is also called washing mark, washing mark, washing cloth, and its materials are: ribbon, Dupont paper, coated tape, woven edge tape, etc.
Embodiment 1
[0028] The printing ink in the present embodiment comprises 0.22% C.I. direct black 168, 2.8% C.I. direct black 19, 0.5% glycerol, 5% 1,3-dimethyl-3-imidazoline by mass percentage ketone, and the balance is deionized water.
[0029] Its preparation method is as follows:
[0030] S1, the mass percentage is 0.22% C.I. Direct Black 168, 2.8% C.I. Direct Black 19, 0.5% glycerin, 5% 1,3-dimethyl-3-imidazolidinone, add deionized water to 100% mix;
[0031] S2. Heat and stir the above mixture at 80°C for 1 hour, cool to 40°C, add 3% ethanol, and continue to stir for 30 minutes;
[0032] S3. Using a membrane with a pore size of 0.4 μm, perform vacuum filtration to obtain the ink for washing the mark.
[0033] Tests and results:
[0034] The physical properties of the above ink at 24°C are as follows: surface tension 33.4Mn / m (measured by BZY-2 automatic surface tension meter), viscosity 3.40cP (measured by R / S coaxial cylinder rheometer), ink particle average The particle size is...
Embodiment 2
[0036] The printing ink in the present embodiment comprises 0.25% C.I. direct black 168, 3% C.I. direct black 19, 0.5% glycerin, 5% 1,3-dimethyl-3-imidazoline by mass percentage ketone, and the balance is deionized water.
[0037] Its preparation method is as follows:
[0038] S1, the mass percentage is 0.25% C.I. direct black 168, 3% C.I. direct black 19, 0.5% glycerin, 5% 1,3-dimethyl-3-imidazolidinone, add deionized water to 100% mix;
[0039] S2. Heat and stir the above mixture at 80°C for 1 hour, cool to 40°C, add 3% ethanol, and continue to stir for 30 minutes;
[0040] S3. Using a membrane with a pore size of 0.4 μm, perform vacuum filtration to obtain the ink for washing the mark.
[0041] To sum up, the pattern printed with the black ink obtained by this method has good quality, is not easy to bleed, does not have rough edges, has good rubbing fastness, has certain light fastness, and the preparation method is simple and economical.
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