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Method for obtaining fine methanol products by using methanol to olefins (MTO) methanol products

A technology for refined methanol and products, which is applied in separation methods, chemical instruments and methods, and the preparation of organic compounds, etc., can solve the problems of increasing public works, large energy consumption, and high cost, and achieves reduced equipment investment, low equipment investment, and equipment The effect of low energy consumption

Active Publication Date: 2015-06-17
SOUTHWEST RES & DESIGN INST OF CHEM IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the low concentration of MTO methanol (its volume concentration is generally lower than 95%), when refined methanol is required, the MTO methanol plant cannot meet the requirements, and MTO methanol needs to be purified, and if a new set of refined methanol plant is built, it will occupy an area and equipment investment, but also need to increase supporting public works
Moreover, to obtain refined methanol by rectification on the basis of the finished MTO methanol, it is necessary to pump the MTO methanol under pressure and reheat it from normal temperature, which consumes a lot of energy and costs too much.

Method used

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  • Method for obtaining fine methanol products by using methanol to olefins (MTO) methanol products
  • Method for obtaining fine methanol products by using methanol to olefins (MTO) methanol products

Examples

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Embodiment 1

[0032] Such as figure 2 Shown: A kind of equipment that utilizes MTO methanol products to obtain refined methanol products, and a set of refined methanol rectification system is added on the basis of the existing MTO methanol three-tower rectification equipment. The equipment specifically includes: a pre-rectification tower 1, a pressurized rectification tower 2, a refined methanol rectification tower 3, and an atmospheric rectification tower 4. The raw material inlet in the middle of the pre-rectification tower 1 is supplied with crude methanol through a pipeline. The system is connected, the tower top outlet of the pre-rectification tower 1 is connected with the exhaust gas treatment system or the fuel pipe network through the pipeline, and the tower still outlet is connected with the raw material inlet in the middle part of the pressurized rectification tower 2 through the pipeline and the booster pump 6 The outlet at the top of the pressurized rectification tower 2 is con...

Embodiment 2

[0036] This embodiment is a flow process with an annual output of 300,000 tons of MTO grade methanol and a by-product of 24,000 tons of refined methanol (see figure 1 ), using equipment such as figure 2 shown.

[0037]Crude methanol flow rate ~ 45900kg / h enters the three-tower rectification system of MTO grade methanol, discharges non-condensable gas from the top of the pre-rectification tower, and produces MTO grade methanol from the top of the pressurized rectification tower and the top of the atmospheric rectification tower. Among them, 18,887 kg / h of MTO grade methanol is extracted from the top of the pressurized rectification tower, and 19,953 kg / h of MTO grade methanol is mined from the top of the atmospheric distillation tower, and the bottom liquid of the atmospheric distillation tower is pumped to the sewage treatment system. The device produced a total of 38.840t / h of MTO grade methanol.

[0038] The content of MTO grade methanol is 95%, which cannot meet the stan...

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Abstract

The invention discloses a method for obtaining refined methanol products by using MTO methanol products, which mainly refers to adding a refined methanol rectification tower in the three-tower rectification process for producing MTO grade methanol products, so as to obtain refined methanol products, satisfying Demand for refined methanol in downstream products. The specific method is: separate a part of the MTO grade methanol product from the top of the MTO methanol pressurization tower, and send it to a refined methanol rectification tower, and obtain the refined methanol product at the top of the refined methanol rectification tower through rectification, while the refined methanol The bottom liquid of the distillation column is returned to the MTO methanol atmospheric column. Through the above steps, the refined methanol product can be obtained with few additional equipment without affecting the production of the original MTO grade methanol product, and the purpose of saving investment can be achieved.

Description

technical field [0001] The invention belongs to the field of chemical industry, and in particular relates to the technical field of methanol preparation and purification. Background technique [0002] With the development of the methanol-to-olefins (MTO) process, the number of domestic MTO methanol plants has increased. Due to the low concentration of MTO methanol (its volume concentration is generally lower than 95%), when refined methanol is required, the MTO methanol plant cannot meet the requirements, and MTO methanol needs to be purified, and if a new set of refined methanol plant is built, it will occupy an area And equipment investment, also need to increase supporting public works. Moreover, to obtain refined methanol by rectification on the basis of finished MTO methanol, it is necessary to pressurize and pump the MTO methanol and reheat it from normal temperature, which consumes a lot of energy and costs too much. Contents of the invention [0003] The purpose ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07C31/04C07C29/80B01D3/14
CPCB01D3/143C07C29/80C07C31/04
Inventor 蹇守华黄维柱陈玲张树杨
Owner SOUTHWEST RES & DESIGN INST OF CHEM IND
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