Ultralow volume liquid containing sulfoxaflor and insect growth regulating pesticide
A technology of ultra-low volume liquid preparation containing sflufenapyr, which is applied in the field of pesticides
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Embodiment 1
[0034] Prepare the ultra-low volume liquid of sulfoxaflor-flubenzuron with a mass percentage of 4.1%, and its components and contents are respectively:
[0035] Sulfoxaflor 4.0 kg
[0036] Flubenzuron 0.1 kg
[0037] N-Methylpyrrolidone 5.0 kg
[0038] Trimethylbenzene 10.0 kg
[0039] Dimethyl phthalate 5.0 kg
[0040] n-octanol 2.0kg
[0041] Penetrant T 0.2kg
[0042] Calcium dodecylbenzenesulfonate 0.5 kg
[0043] Castor oil polyoxyethylene ether 0.5kg
[0044] The second-line oil is supplemented to 100 kg.
[0045]The preparation process is as follows: in a stirred reaction vessel, first stir and dissolve sulfoxaflor and imidacloprid with a solvent, then add auxiliary ingredients, stir and mix evenly, and then obtain 4.1% sulfoxaflor. Urea ultra-low-capacity liquid agent; the process parameters are: the stirring speed is controlled at 60-150 rpm, the stirring time is 15-60 minutes, the temperature is normal temperature, and the pressure is normal pressure.
[004...
Embodiment 2
[0048] Prepare the ultra-low volume liquid of sulfoxaflor-flubenzuron 4 with a mass percent content of 8.1%, and its components and contents are respectively:
[0049] Sulfoxaflor 0.1 kg
[0050] Flubenzuron 8.0kg
[0051] N,N-Dimethylformamide 5.0 kg
[0052] N-Methylpyrrolidone 5.0 kg
[0053] n-octanol 3.0kg
[0054] Benzyl alcohol 2.0kg
[0055] Azone 0.2 kg
[0056] 2-butyl acetate 8.0kg
[0057] Calcium dodecylbenzenesulfonate 2.0 kg
[0058] Alkylphenol polyoxyethylene ether 3.0kg
[0059] Phenylphenol polyoxyethylene ether 0.5kg
[0060] Soybean oil supplemented to 100 kg.
Embodiment 3
[0062] The preparation mass percentage composition is 15% sulfoxaflor-flubenzuron ultra-low volume liquid, and its composition and content are respectively:
[0063] Sulfoxaflor 5.0 kg
[0064] Flubenzuron 10.0kg
[0065] N-Methylpyrrolidone 8.0 kg
[0066] N,N-Dimethylacetamide 10.0 kg
[0067] Acetophenone 6.0 kg
[0068] Epoxidized soybean oil 4.0 kg
[0069] o-dichlorobenzene 6.0 kg
[0070] Azone 0.3 kg
[0071] Calcium dodecylbenzenesulfonate 2.0 kg
[0072] Octylphenol ethoxylate 2.5 kg
[0073] Alkylarylpolyoxypropylene polyoxyethylene ether 1.0 kg
[0074] Turpentine Make up to 100 kg.
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