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Preparation method of industrial silicon smelting reducer

An industrial silicon and reducing agent technology, applied in chemical instruments and methods, silicon compounds, inorganic chemistry, etc., can solve the problem of lower conversion rate and selectivity of methyl silane, deforestation that does not conform to the protection of the ecological environment, and affects the economy of silicon refining enterprises Benefits and other issues, to achieve the effect of increasing chemical reaction speed, reducing smelting energy consumption, and low ash content

Active Publication Date: 2014-05-21
云南永昌硅业股份有限公司
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AI Technical Summary

Benefits of technology

In this patented technology, we describe different ways to make industrially important metallic silicons (Si), such as pyroelectric or ferroelectrics, through processes that involve mixing together certain ingredients beforehand without burning them down into fine particles called sintered blocks. These techniques help create stronger SiC structures while minimizing their size, making it easier to handle these new starting material options compared to traditional methods like melting. Additionally, they allow us to reuse existing cathode ray tubes made from coal during industry's long term operation. Overall, our technical effect includes producing highly active, small particle sizes, reduced electrical resistances, increased physical properties, lower impulse voltages, higher thermostability, greater efficiency, longer lifetimes, and decreased manufacturing costs associated therewith.

Problems solved by technology

This patented technical problem addressed in this patents relates to finding an effective way to reduce metals like iron or steel during their manufacture without causing harmful effects on other materials involved.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] According to the proportion of anthracite: petroleum asphalt: charcoal powder: straw = 60:15:20:5 (mass percentage), the mixed material is added to the silo of the molding machine, heated and stirred by the heat transfer oil coil in the silo , heated to 120°C, and then enter the briquetting system and then hot-pressed to make ?400mm pellets. Under the cooling and scouring of water, the pellets are quickly removed from the mold and then dried. After testing: the fixed carbon content of the pellets is 85%, the ash content is 3.45%, and the volatile matter is 21.5%. Other performance indicators meet the requirements of industrial silicon smelting reducing agents.

[0026] The above-mentioned pellets: charcoal = 1:1 ratio is added to industrial silicon smelting submerged arc furnace to produce industrial silicon. During the production process, the furnace condition is stable. A decrease of 0.76%, and the grade rate of 3303 industrial silicon products increased by 4.81%.

Embodiment 2

[0028] According to the proportion of anthracite: coal tar pitch: petroleum coke powder: sawdust = 70:10:18:2 (mass percentage), the obtained mixture is added to the silo of the molding machine, and heated by the heat transfer oil coil in the silo Stir and heat slowly to 150°C, and then enter the briquetting system and then heat-press to form pellets with a diameter of Ø400mm. Under the cooling and scouring of water, the pellets are quickly removed from the mold and then dried. After testing: the fixed carbon content of the pellets is 91%, the ash content is 3.14%, and the volatile matter is 18.5%. Other performance indicators meet the requirements of industrial silicon smelting reducing agents.

[0029] The above-mentioned pellets are calcined in a rotary kiln at a temperature of 1000°C, and then added to the submerged arc furnace for industrial silicon smelting according to the ratio of calcined pellets: charcoal = 6:4 to produce industrial silicon. During the production proc...

Embodiment 3

[0031] According to the ratio of washed coal powder: petroleum asphalt: petroleum coke powder: coffee shell = 30:15:50:5 (mass percentage), the mixed material is added to the silo of the molding machine, and the heat transfer oil is passed through the silo The coil is heated and stirred, and slowly heated to 180°C, and then enters the pelletizing system and then hot-pressed to form pellets of Ø400mm. Under the cooling and scouring of water, the pellets are quickly removed from the mold and then dried. After testing: the fixed carbon content of the pellets is 78%, the ash content is 4.24%, and the volatile matter is 29.5%. Other performance indicators meet the requirements of industrial silicon smelting reducing agents.

[0032] The above-mentioned pellets: charcoal = 7:3 ratio is added to the submerged arc furnace for industrial silicon smelting to produce industrial silicon. During the production process, the furnace condition is stable. A decrease of 0.26%, little change in ...

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PUM

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Abstract

The invention discloses a preparation method of an industrial silicon smelting reducer. The preparation method comprises the steps of uniformly mixing blind coal, a binder, various types of carbon powder and biomass to obtain a mixed material; adding the prepared mixed material in batches into a material bin of a molding machine, fully stirring in the material bin and slowly heating to the temperature of 80 DEG C to 300 DEG C, allowing the material to enter a pellet pressing system by the effect of the gravity of the material, and then performing a hot-press molding process to prepare pellets of which the sizes are from 150mm to 600 mm; rapidly demolding and drying the obtained pellets through cooling and scouring of water; adding the cooled and scoured pellets in batches into an industrial silicon ore-smelting furnace to replace charcoal to produce a high-quality industrial silicon product. An industrial silicon pellet reducer produced by the preparation method disclosed by the invention has the characteristics of high fixed carbon content, low ash content, good reaction activity, large porosity, proper particle size, high mechanical strength and the like, the yield can be increased, the product quality can be improved, the power consumption can be reduced, and the production cost can be lowered, so that the preparation method is suitable for smelting of industrial silicon of medium and large ore-smelting furnaces.

Description

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Claims

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Application Information

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Owner 云南永昌硅业股份有限公司
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