Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Production method of hot-rolled 409l ultra-pure ferritic stainless steel strip by annealing and pickling

A technology for stainless steel strips and production methods, applied in metal rolling, metal rolling, workpiece surface treatment equipment, etc., can solve the problems of insufficient pickling, low surface quality, and inability to effectively remove scale on the surface of strip steel, etc., to achieve improved Yield and effect of improving surface quality grade

Active Publication Date: 2016-08-17
WISDRI ENG & RES INC LTD
View PDF2 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The production method currently used, because the hot-rolled ultra-pure 409L ferritic stainless steel surface oxide scale is closely combined with the metal matrix, the strip steel surface oxide scale is not cleaned during the pickling process, and the strip steel surface roughness after pickling is relatively high. Large, the surface quality of strip steel after pickling is low, and often cannot meet the surface quality requirements of NO.1 products
[0003] At present, after annealing and mechanical descaling, when hot-rolled 409L ultra-pure ferritic stainless steel strip is pickled, sulfuric acid pre-pickling + mixed acid pickling process is generally used, because the oxide scale on the surface of 409L strip steel is closely combined with the metal matrix , Sulfuric acid pre-pickling cannot effectively remove the scale on the surface of the strip, and the pickling effect of mixed acid on 409L is poor, resulting in frequent under-pickling

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment approach

[0027] The technical scheme of the present invention has more optimized implementation mode as follows:

[0028] More optimally, the elongation rate in step 1) is controlled between 0.8% and 1.2%; then the shot blasting machine is descaled, the shot blasting volume is 830 ~ 870kg / min, and the speed of the shot blasting machine is between 1750 ~ 1850rpm.

[0029] More optimally, in step 2), the concentration of sulfuric acid solution is 140g / L-160g / L, the concentration of metal ions is 45-55g / L, the temperature of the acid solution is between 65-75°C, and the current is between 875-925A. The strip speed is between 55-65m / min.

[0030] More optimally, the sulfuric acid concentration in step 3) is between 240-260g / L, the metal ion concentration is 45-55g / L, the acid solution temperature is between 75-85°C, and the strip speed is between 55-65m / min between.

[0031] More optimally, in step 4), the concentration of nitric acid is between 70-90g / L, the concentration of hydrofluori...

Embodiment 1

[0034] The annealed steel strip is descaled by a scale breaker, and the elongation is controlled to 0.8%; then descaled by a shot blasting machine, the shot blasting volume is 830kg / min, and the shot blasting machine speed is 1750rpm;

[0035] The strip after shot blasting and descaling passes through a sulfuric acid electrolytic pickling tank, in which the concentration of sulfuric acid in the tank is 140g / L, the concentration of metal ions is 45g / L, the temperature of the acid solution is 65°C, the current is 875A, and the strip speed is 55m / min;

[0036] Go through a sulfuric acid electrolytic pickling tank and pass through a sulfuric acid pickling tank, the concentration of sulfuric acid in the tank is 240g / L, the concentration of metal ions is 45g / L, the temperature of the acid solution is 75°C, and the strip speed is 55m / min;

[0037] After sulfuric acid pickling, it passes through the mixed pickling tank, the concentration of nitric acid in the tank is 70g / L, the concen...

Embodiment 2

[0041] The annealed steel strip is descaled by a scale breaker, and the elongation is controlled to 1.2%; then descaled by a shot blasting machine, the shot blasting volume is 870kg / min, and the shot blasting machine speed is 1850rpm;

[0042]The strip after shot blasting and descaling passes through a sulfuric acid electrolytic pickling tank, in which the concentration of sulfuric acid solution in the tank is 160g / L, the concentration of metal ions is 55g / L, the temperature of the acid solution is 75°C, the current is 925A, and the speed of the strip steel is at 65m / min;

[0043] After passing through a sulfuric acid electrolytic pickling tank, it passes through a sulfuric acid pickling tank, the concentration of sulfuric acid in the tank is 260g / L, the concentration of metal ions is 55g / L, the temperature of the acid solution is 85°C, and the strip speed is 65m / min;

[0044] After sulfuric acid pickling, it passes through the mixed pickling tank, the concentration of nitric ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
widthaaaaaaaaaa
thicknessaaaaaaaaaa
elongationaaaaaaaaaa
Login to View More

Abstract

The invention discloses a hot-rolled 409L ultra-pure ferrite stainless band steel annealing and acid-pickling production method, which comprises the following steps: performing scale breaking to the annealed band steel through a scale breaker; then carrying out scale removal through a shot blasting machine; flowing through a sulfuric acid electrolysis pickling bath; flowing through a sulfuric acid pickling bath after the sulfuric acid electrolysis pickling bath; flowing through a mixed acid pickling bath; flowing through a nitric acid pickling bath after being pickled by mixed acid, wherein the concentration of nitric acid in the bath ranges from 60g / L to 100g / L, the concentration of metal ions ranges from 5g / L to 20g / L, the temperature of acid ranges from 30DEG C to 45DEG C, and the speed of the band steel ranges from 50m / min to 70m / min. By effectively regulating the annealing temperature, band steel speed, elongation rate, the shot blasting quantity of the shot blasting machine, as well as the rotating speed, acid-pickling technology, current size, acid concentration, acid temperature and acid ingredients, the oxide scale on the surface of the band steel can be thoroughly removed, the grade of acid-pickled surface quality of the band steel can be improved, excellent surfaces can be obtained and the material yield can be increased.

Description

technical field [0001] The invention belongs to the field of stainless steel production, in particular to a production method for annealing and pickling hot-rolled 409L ultra-pure ferritic stainless steel strip. Background technique [0002] During the finishing rolling process of hot-rolled ultra-pure 409L ferritic stainless steel strip steel, a dense oxide layer will be formed on the surface of the strip steel. After annealing in a continuous annealing furnace, the thickness of the oxide layer will become thicker. , it is necessary to use a scale breaker and a shot blasting machine to remove most of the scale on the surface of the strip, and then go through sulfuric acid pre-pickling + mixed acid pickling process to remove the scale on the surface of the strip and form a dull layer on the surface of the strip. film. The production method currently used, because the hot-rolled ultra-pure 409L ferritic stainless steel surface oxide scale is closely combined with the metal m...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C25F1/06B21B45/06
Inventor 李勇华胡斯尧陈连龙
Owner WISDRI ENG & RES INC LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products