Binary carbon material-conductive polymer composite nanometer gas-sensitive film and preparation method thereof
A technology of conductive polymer and binary carbon material, applied in the field of composite nanomaterials and thin film technology, can solve the problems of poor selectivity and stability of single carbon material gas sensitive thin film, achieve excellent gas sensitive performance and enhance electrical conductivity and gas-sensing characteristics, the effect of simple preparation process
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[0055] ①Using the gold interdigitated electrode as the substrate; the substrate was ultrasonically cleaned in acetone, ethanol and deionized water for 10 minutes, and dried with nitrogen;
[0056] ②Place the substrate in a volume ratio of 1:1:5 ammonia water / hydrogen peroxide / water solution for 30 minutes to make the surface of the substrate hydrophilic;
[0057] ③Take 2ml of polydiallyl ammonium chloride (PDDA) standard solution with a concentration of 20%wt, prepare 40ml of polycationic electrolyte PDDA aqueous solution with a concentration of 1%wt, and ultrasonicate for 10min for later use; take 0.1g of poly(p-styrene Sodium sulfonate) (PSS), add 47.5ml of deionized water and 2.5ml of 2mol / L hydrochloric acid solution to make polyanion electrolyte PSS aqueous solution, ultrasonic for 10min for later use;
[0058] ④Weigh 0.5mg of graphene nanosheets and single-walled carbon nanotubes respectively, add 5ml of deionized water to prepare the aqueous dispersion of binary carbon ...
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