Recycling method for phthalic anhydride residues
A technology of residue and phthalic anhydride, which is applied in the field of recycling and utilization of phthalic anhydride residue to achieve high recovery rate and reduce emissions
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[0012] In the following, the present invention will be further described in conjunction with the embodiments:
[0013] Such as figure 1 Shown:
[0014] The specific steps for recovering di-n-butyl phthalate from phthalic anhydride residue are as follows:
[0015] 1) Grinding and screening of phthalic anhydride residue: After being milled by ball mill 1, the phthalic anhydride residue is put into ball grinding tank 2. The powder of the ball mill is lifted to rotary vibrating screen 4 by elevator 3 for sieving. The particle size of phthalic anhydride residue is l~5mm;
[0016] 2) Esterification: Under stirring, 74 grams of phthalic anhydride residue powder and 155 grams of n-butanol are added to the esterification reactor 7 for esterification, and the n-butanol is passed from the n-butanol storage tank 5 through the n-butanol feeding pump 6 Put into the esterification reactor 7, and at the same time add 2.22 grams of catalyst sulfuric acid to the esterification reactor, the esterifica...
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